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Heroin testing protocol

G.Patton

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Introduction

You bought strange heroin product and want to carry out pollution and admixture testing experiments before using. Use this article as a guide for experimenting. Here the list of manipulations with heroin is performed, useful information for home tests and product brief.
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Forms

It is a semisynthetic opiate made by extracting morphine from the opium produced by opium poppies and then acetylating the morphine into diacetylmorphine (heroin). Pure heroin looks like a white powder and may be smoked or snorted. Darker, more impure heroin is diluted or dissolved, and then injected into one’s skin, muscles, or veins. Street heroin is almost never pure. It may be a white powder or dark brown. The consistency can vary widely as there may be many impurities depending on the manufacturing process. Sugars, starches, powdered milk, and even other types of drugs may be added as filler. The unpredictable strength of the drug further complicates matters on top of the person’s addiction to it.

Hydrochloride salt.
Heroin, also known as diacetylmorphine and diamorphine among other names, is an opioid used as a recreational drug for its euphoric effects. Medical grade diamorphine is used as a pure hydrochloride salt which is distinguished from black tar heroin, a variable admixture of morphine derivatives—predominantly 6-MAM (6-monoacetylmorphine), which is the result of crude acetylation during clandestine production of street heroin.
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Black tar heroin.
Black tar heroin is a free base form of heroin that is sticky like tar or hard like coal. Its dark color is the result of crude processing methods that leave behind impurities. Despite its name, black tar heroin can also be dark orange or dark brown in appearance. It is generally less expensive than other forms of heroin.

Black tar heroin is impure diamorphine. Other forms of heroin require additional steps of purification post acetylation. With black tar, the product's processing stops immediately after acetylation. Its unique consistency, however, is due to acetylation without a reflux apparatus. Black tar as a type holds a variable admixture of morphine derivatives—predominantly 6-MAM (6-monoacetylmorphine), which is another result of crude acetylation. The lack of proper reflux during acetylation fails to remove much of the moisture retained in the acetylating agent, glacial acetic acid.
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The most popular admixtures of heroin

Depending on how it is processed, it ranges from a thick sticky "black tar" to a brown, tan, or white powder. Street material varies greatly in potency, from as high as 90% purity to as low as 5 or 10% purity. Heroin is most commonly injected (intravenously, intramuscularly, or subcutaneously), smoked, or insufflated (snorted). Pure morphine and heroin are both fine powders. Tar's unique appearance and texture is due to its acetylation without benefit of the usual reflux apparatus.

The assumption that tar has fewer adulterants and diluents is a misconception. The most common adulterant is lactose, which is added to tar via dissolving of both substances in a liquid medium, reheating and filtering, and then recrystallizing. This process is very simple and can be accomplished in any kitchen with no level of expertise needed.

Most common pollutants of heroin are 6-monoacetylmorphine (product of incomplete acetylation), codeine, 6-Acetylcodeine papaverine, hydrocotamine. Also, very common synthetic adulterants are found such as caffeine, dextromethorphan (DXM), dipyrone, aminopyrine, a-PVP, ketamine, amphetamine, methamphetamine, fentanyl, 4-ANPP, diphenhydramine, procaine, quinine, lactose and maltose, mannitol and so on. There is a list of heroin analysis reports in the USA drug analysis laboratory.

Heroin is often “cut” (diluted/mixed) with fentanyl or fentanyl derivatives/analogs (4-fluorofentanyl, 4-ANPP, carfentanil) in order to enhance the effect of the drug. But recent reports have proven this to be an extremely dangerous combination. Cutting heroin with fentanyl increases the potency of both substances, which are already very strong as stand-alone drugs. And because fentanyl is significantly more potent than heroin, mixing the two can cause a more severe opioid-induced intoxication and greatly increase the risk of death.
According to a spokesperson from the U.S. Drug Enforcement Administration (DEA), it takes very little to dangerously overdose on fentanyl, and amplifying the potency of fentanyl with heroin can be fatal.

Algorithm of procedures:

1. Firstly, I strongly recommend determining fentanyl or fentanyl derivatives/analogs using special Fentanyl test kit which is containing test stripes. This substance extremely dangerous, especially in a pair of heroin. If you find this substance, I recommend you to get rid of your impure heroin to safe your life. You cannot measure the amount of fentanyl in your heroin product by any improvised means and cannot define safety dose. There are information about LF tests (drug testing kits).

How to test it?

A: Choose your option.
Option 1:

  • Dissolve all the drugs you plan to use in water by following the instructions in Step B.
  • This is the most accurate way to test your drugs, since fentanyl is not always mixed evenly throughout. If you cannot test your drugs this way, try Options 2 or 3.
  • After testing your drugs this way, you can drink them, snort them using a clean nasal spray device or wait until the water evaporates to use them.
Option 2
  • Finely crush your drugs on a clean surface.
  • Put the crushed drugs in a small, plastic bag and shake the bag to mix them.
  • Empty the bag and put your drugs to the side. A small amount of drug residue should be left in the bag.
  • Add water to the bag by following the instructions in Step B.
Option 3
  • Put 10 milligrams (mg) of your drugs (enough to cover Abraham Lincoln’s hair on a penny) in a clean, dry container.
  • If you cannot test 10 mg of your drugs, put at least a few grains in a clean, dry container.
  • Add water to the container by following the instructions in Step B.
B: Add water.
  • Add water to your drugs and mix them up.
  • Use half teaspoon of water for every 10 mg of crystal or powder you are testing.
C: Use the test strip.
  • Place the test strip with the wavy side down in the water. Let the strip absorb the water for 15 seconds.
  • Take the strip out of the water and place it on a flat surface for two minutes.
  • Read the results (see “What do the test results mean?”).
  • Tips for testing your drugs:
  • Do not use test strips more than once.
  • Finely crush pills and tablets, add water to the powder and mix thoroughly. If you do not want to test the entire pill, break it in half and test a portion from the middle.
What do the test results mean?
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The fentanyl testing strips are capable of detecting a dozen different fentanyl family members, and there isn’t a single one of them that isn’t life-threatening or dangerous to your health. The members are:
  • 3-Methylfentanyl,
  • 4-Fluorofentanyl,
  • Acetylfentanyl,
  • Alfentanil,
  • Butyrfentanyl,
  • Carfentanil,
  • Fluoroisobutyrfentanyl,
  • Furanylfentanyl,
  • Ocfentanil,
  • Remifentanil,
  • Sufentanil,
  • Thiofentanyl.
2. Secondary, you have to provide visual checking of your heroin. If the product has visible inorganic pollutants such as sand, paper, plastic/glass/wood particles and so on, you have to filter your product through a paper filter (coffee machine filter is suitable). Also, I recommend providing Heroin purification before next stages of testing. Although fentanyl and its analogues were identified in the first step, your product may contain other hazardous substances described above.

3. Thirdly, confirm the compliance of the product with heroin by LF tests (drug testing kits). You will receive clear result about your substance and admixtured narcotic substance (if it takes place to be) and these tests help to choose next step.

4. After purification procedure, heroin powder should be lighter and less colored. For determine caffeine, you may use same method with nitric acid and ammonia solution as for amphetamine.

5. Next, if any pollutants are not found or LF tests (step 3) reveal admixtured narcotic substance, you have to check your heroin sample with test reagents. Use «Drugs testing reagents». These methods help to determine kind of admixtures. There are manuals, which are described checking method procedures and meaning, where you can find methods of reagent synthesis. In case of heroin TLC experiments may be rather hard for interpretation by means that usually heroin contain mixture of substances such as 6-monoacetylmorphine, codeine, 6-Acetylcodeine papaverine, hydrocotamine and some opiates. This mixture will split on TLC plate and hinders heroine pollutants detection.

For instance, you place heroin sample (couple lump) into a small white/colorless plate or Petri dish. Add two drops of Mecke reagent and observe the reaction.
  • If the reaction has bluish green color after 60 seconds, it means you have the pure heroin sample.
  • If the reaction has orange color, it means your heroin is polluted by dextromethorphan. This substance is quite often identified in heroin products.
Also, carry out experiment with Mandelin reagent. In addition, couple drops of reagents, you may observe following reactions:
  • If the reaction has deep brown color after 60 seconds, it means you have the pure heroin sample.
  • If the reaction has deep reddish orange color, it means your heroin is admixtured by ketamine. This substance meets sometimes in street heroin analysis reports.
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I would recommend providing tests with several reagents because you can have a mixture of admixtured drugs in the sample, testing results may show a mix of colors. Different test reagents allow interpreting results of testing more clearly.

Conclusion

Melting point verification can be added to the third step to confirm quality compliance and to determine the degree of impurity content. The best ways to determine composition of heroin mixture are GC-MS or LC-MS analysis. However, this manual allows identifying most number of heroin impurities and approve results by different methods.
 
Last edited:

None

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Hello brother, I need your help
I have a few questions, I produced heroin but it has no power, it is very weak, I will tell you how to do it, show me
I extracted morphine with calcium oxide, then evaporated with ammonia, then boiled with a small amount of hydrochloric acid and charcoal, filtered, then refluxed with acetic acid for 6 hours, treated the liquid with sodium hydroxide, then extracted with chloroform. And I evaporated. It is not strong at all, where is the problem
 

G.Patton

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Hello brother, I need your help
I have a few questions, I produced heroin but it has no power, it is very weak, I will tell you how to do it, show me
I extracted morphine with calcium oxide, then evaporated with ammonia, then boiled with a small amount of hydrochloric acid and charcoal, filtered, then refluxed with acetic acid for 6 hours, treated the liquid with sodium hydroxide, then extracted with chloroform. And I evaporated. It is not strong at all, where is the problem
NoneHello, this topic isn't appropriate for your question. Write there : Synthesis of Heroin from opium raw
P.S. Read this correct extraction method.
 

None

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The next question, I have a problem with titration. I use an acidic solution of 100 cc with baking soda (sodium hydroxide) in order to make it acidic or to titrate the solution to one liter. Because I mix the soda with water, use it like this. Chloroform rises in the decanter, what should I do?
 

G.Patton

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The next question, I have a problem with titration. I use an acidic solution of 100 cc with baking soda (sodium hydroxide) in order to make it acidic or to titrate the solution to one liter. Because I mix the soda with water, use it like this. Chloroform rises in the decanter, what should I do?
NoneI'm sorry, but you write something not related to real chemistry. Baking soda is NaHCO3. It makes a solution basic, not acidic... Do you know what is titration? For what reason do you carry out it?
 

None

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Thanks for the answer, I'm talking to you with Google Trans, the words are moved, the meaning changes. I also know that baking soda is playing, but I can't convey my meaning.
 

41Dxflatline

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Baking soda, "bicarb" = sodium bicarbonate
Baking powder,= baking soda and an acid salt buffered with cornstarch. reacts when wet to create carbon dioxide to leven baked goods
Washing soda, = sodium carbonate, can be made from bicarb by baking it.

Unslaked/burnt/quick lime = calcium oxide. Can be mixed with water to create calcium hydroxide, aka slaked lime.
Lye = usually sodium hydroxide, sometimes postassium hydroxide. Both are nearly entirely interchangable in practice. A weak potassium hydroxide solution can be made from wood ashes mixed with water, this is called "wood ash lye"

Ammonia or "household ammonia" a solution of ammonia in water smells like stale piss and is basically a very localised chemical weapon. Don't mix with bleach unless you want a field tested chemical weapon to form (chlorine gas)
Bleach is sodium hypochlorite,sometimes mixed with a surfactant if it's 'thick toilet beach' like domestos

Those are all the household bases and their names
 
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