Reaction scheme:
Synthesis:
Methanesulfonic acid (MSA, 288g) and propionic anhydride (156g) were charged into a 1 liter reaction flask.
The mixture was cooled to 0°C, and 122g of 3,4-methylenedioxybenzene (MDB) was added under stirring.
The reaction mass was maintained at 0°C to 5°C for 4...