>O,O-Dibenzoyl-2R,3R-Tartaric Acid
I think it is much hard to find than d-tartaric acid
Sorry, I was confused. L(+) isomer can be used to get (-)D-amph/methamph. Procedure a little bit different from mine and you can get another isomer. I worked with D-Isomer only. You'll get D-amph L-tartaric acid as an precipitate.
So can we then take this tartrate salt D-Amph L-Tartaric, treat with sodium hydroxide, extract and precipitate with with sulphuric acid?
Acetic essence is often used to produce hydrogen, but I "start" the reaction to produce hydrogen with water. Less acidic medium, which means less alkali must be added later.
In this method is not used acetic acid, but is used another chemical together with p2np in a solution, is that the difference compared to the method used in the 2 videos to make amphetamine from aluminum amalgam?
can somebody explain me again pls what would be the difference if I use l-tartaric instead of d-tartaric acid with freebase? with l-tartaric there would precipate what? the d-amphetamine l-tartaric salt? What would I do then?
with L-(+)-tartaric acid it means you will have dextro amphetamine salt crystallizing or levo? sorry its very confusing.
"You can repeat procedure of cleaning precipitate of l-amphetamine d-tartaric salt by methanol to increase yield."
I want to do that. Can you describe the steps in more detail?
Question about p2np to amph.
So I used aluminium granules as I had that laying around.
After I amalgamated it which was deep grey sludge floating around I drained and wash 4 or 5 times added small amount of distilled water and dripped 14%p2np in ipa slowly at 1st but my exotherm wasn't bad 45°c'ish I speeded it up but even after all addition in about 15mins it never went over 55c without cooling, I don't think enough hydrogen was produced from the slow reaction. Could I bubble h2 through mixture from hydrogen generator to make sure I'm using enough hydrogen or have I just fucked it up with granules?
Just wanted to know before I basify
It is better to use Al foil from grocery store for this synthesis way. In case of H2 bubbling, it is better to use Pd/C as catalyst.
I've tried to look but can't really find an answer for pd/c preparation
I have activated carbon and maybe 50g of palladium chloride made by dissolving palladium in aqua rega and bubbling chlorine through which dropped out a nice dark red salt looks a little like iron oxide. And dried to constant weight.
How do I make pd/c
Sorry a bit off topic.
Is pd/c pyrophoric?
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