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papaji

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Done with good quantity of mephedrone anyone is here to help ???
This product has burning sensation in eyes and also have burning taste in mouth anyone's here to help me to get out this rid
 

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papaji

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Yes i did purification procedures one is from ethyl acetate which removes almost 60% impurities after that i used syringe wash of product from isopropanol but still that product have some impurities so i recrystallization from isopropanol but this product still has burning taste in mouth and whenever it's snorted by nose it burns in nose and eyes got tears i can't use acetone because of i dont have a freezer which can give temprature to-15°c so my product almost dissolves in dry acetone do you have any further solution regarding to it please suggest me brother ????
 

papaji

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Same problem iam also facing. In fact the final product is bringing tears to eyes and is burning on tongue
vig212Did you get rid out of this problem if yes then how ???
 

Venom2021

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why the filmmaker says that the efficiency of 4mmc powder is 100g + with 2b4m ?? who's lying ?? :(
 

Venom2021

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with 100g 2b4m the filmmaker receives 100g +/- 4mmc not real yield 60g / 80g this is more real output 4mmc
 

G.Patton

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Nnn

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The reaction with NMP takes 15-20 minutes, it can be replaced by Dimethyl sulfoxide, Dimethylformamide or Sulfolane.
But NMP is the best choice.
For 1g of 2-bromo-4-methylpropiophenone you take 3ml of benzene, if not completely dissolved you can add 1-2ml. The reaction takes much longer in benzene. If you don't heat the mixture, reacts for ~24 hours, depending on the amount of ketone.
Marvin Popcorn SuttonIf we hav taken 2b4m how much time taken dissolves in NMP and heating degree also.
 

tony rider

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Where to buy N-methylpyrrolidone?
I searched for vendors on the forum but found none. Tnx
 

Venom2021

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if you want to make a very good 4mmc, bk4dcm and methylamine for amination are enough Benzene is carcinogenic and also not necessary for synthesis. guys have nice syntheses but too much fun in them and you won't get high scores
 

Venom2021

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Cristal what I'm get ♡
 

rafael1985

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Done with good quantity of mephedrone anyone is here to help ???
This product has burning sensation in eyes and also have burning taste in mouth anyone's here to help me to get out this rid
papajiMaybe You put to much HCL or all ketone was not react
 

Venom2021

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You put more hcl to pH 4or 3 is no problem you must get powder 4mmc
 

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diogenes

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if you want to make a very good 4mmc, bk4dcm and methylamine for amination are enough Benzene is carcinogenic and also not necessary for synthesis. guys have nice syntheses but too much fun in them and you won't get high scores
Venom2021What do you mean by high scores? High yield? Do you know a good source for BK4dcm? thanks
 

Venom2021

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Yes my good friend made a lot legal bk4
I'm say form 100g bk4 you get 60g to 75g 4mmc cristal
 

dedhy

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What can be used instead of Hydrochloric Acid 35%? Can't get more than 10%, if I'm lucky.
Also, is it possible to increase concentration of methylamine aq sol from 38% to 40%? Is 2% critical for this synthesis?
 

Bazooka90

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If we hav taken 2b4m how much time taken dissolves in NMP and heating degree also.
NnnHow about toluen,i put 300ml per 100g of 2b4m and my final yield was 10g of 4mmc.How much time i must let 2b4m in toluen to react and how much temperature?
 

rafael1985

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I hear with NMP it is 15 min stirring and reaction come
 
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