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Bigwest

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I have all the ingredients, i am trying to Split the 8 & 4 minutes of irradiation on 2 by 2 minutes and let thé product cooled between them but its not working. Could somone help with that pls.
 

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I have all the ingredients, i am trying to Split the 8 & 4 minutes of irradiation on 2 by 2 minutes and let thé product cooled between them but its not working. Could somone help with that pls.
BigwestYou can try to split it to 10-25 sec. Don't cool them too much.
 
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Bigwest

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Are you sure in your reagents? Have you checked their mp?
G.PattonHi
I did check all the melting points of my raw material. Evry thing its OK. Have you try this synthesis by à household microwave ?

I think its not gonna working. it Just can be done by a mw reactor only
 

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Hi
I did check all the melting points of my raw material. Evry thing its OK. Have you try this synthesis by à household microwave ?

I think its not gonna working. it Just can be done by a mw reactor only
BigwestHi, I didn't. I asked about this synthesis for you from William. Ty for your feedback.
 

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Hello.. Just a little explication pleas.
How long should we irradiate the product when using a home microwave---8--4 minutes or 10---25-- seconds? And does the cup have to be closed?
 

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Do we use 400w also in household microwave ?
 

41Dxflatline

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If microwaves work then so should ultrasound
 

Alex7920

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What type of microwave is good for this reaction? Can this reaction be done with a home microwave?
 

joejoe354354

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Hello,I would like to ask if this method is nof suitable for mass production?
 

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Hello,I would like to ask if this method is nof suitable for mass production?
joejoe354354This may only be possible with the aid of a flow type MW reactor that can be conceived as improvisable from a household device but needs someone with quite some experience and balls.
 
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