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powder addition funnel? any idea??

TotalSynthesis

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Hi together,

does anybody know if something like a powder addition funnel does exist? I've never seen it.
Or any good idea how to construct one?

I#d like to add pellets of dry ice to a going reaction which is too nasty to open the reaction vessel for the addition. And i also cant give it through the condensor
 

G.Patton

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I mean conventional funnel with a wide neck in my descriptions to syntheses
L5Oh2Dwbkm
 

TotalSynthesis

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thank you Patton!

But still, this is not a closed system.
I still have to remove the plug from the second neck and switch it with this one and then the reverse procedure again.

well, i guess i need to improvise and build something myself
 

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I still have to remove the plug from the second neck and switch it with this one and then the reverse procedure again.
TotalSynthesisYes, you can do it quite fast. If there is no vacuum, it shouldn't be a problem.Because another option is this funnel. But it isn't appropriate for dry CO2 pellets unfortunately. You can cold your reaction externally.
7avLUFSQWw
 
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