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Preperation of 40% aqueous methylamine solution

reggiesaws

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Hi. Can someone please advise the best and safest way to prepare a 40% aqueous methylamine from methylamine HCL? What are the safety precautions when doing this.
 

Mr.Blanks00

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Hi. Can someone please advise the best and safest way to prepare a 40% aqueous methylamine from methylamine HCL? What are the safety precautions when doing this.
reggiesaws
.by immersing the methylamine vapor in cold water 5-10 degrees, if so then you need to calibrate it a bit by adding hcl and then vaporizing it and getting the reading.
 

Mr.Blanks00

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Hi. Can someone please advise the best and safest way to prepare a 40% aqueous methylamine from methylamine HCL? What are the safety precautions when doing this.
reggiesawshow to make it by adding a concentrated solution of naoh in methylamine hcl and heating slowly to a temperature of 60% and the steam is run with a hose in a cold water solution.
 

T0lek511

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Just add NaOH and the methylamine gas keep bubbling trought distiled water and by weight and by volume you can find % of your solution. And if its higher then 40% just add water.
 
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