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Can acetone be replaced by IPA?
Large glass reactors, or equipped plastic barrelsWhat equipment is used for large scale production?
Yes, but in small quantities. Otherwise, you will have to evaporate alcohol.
Large glass reactors, or equipped plastic barrels
methylene chloride is better in my opinion at 4mmc true 2h 40 ° but with 40 ° taulen it is too small the temperature must be higher than 50%, i.e. 100g bk4 50g 4mmc + a lot of impurities because you do not clean the oil at all I see after crystallization you will have somewhere 40g maybe less efficiency I obtained 70% and 80% yield on methylene chloride
you're right. After crystallization, I was left with 40%. And when I tried to salt the solution with caustic soda once, I had 23% efficiency left.
As for chloromethane, at 40 ° C, two layers separated with stirring for two hours. However, after 10 minutes, the color was the same and there were no two layers. Can I also use chloromethane in 3cmc?
Maybe You put to less methylamine.
For 1 kg ketone nie much You give methylamine?
Here is the result of the 3cmc
Can You tell how You make powder You put cold acetone HCl and let on freezer ?
I didn't give to freezer. I waited and the substance will dry out which took time. Then I rinsed with acetone and there was powder. I did according to my own recipe. Now I want to try 3cmc with a refrigerator to speed up the process
With 3 cmc you will be have more fun
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