troubleshooting jwh synth

[Selassi]

Hey guys
I tried the jwh018 synth exact the same way as the ur-144.

Now in the last step after seperation of the oil in the siliconemolds, here the oil doesnt crystallize but stays a thick viscous oily consistancy...

Anyone seen this before or know what next?

 

[Selassi]

Here is how it looks

 

[HIGGS BOSSON]

It looks like oil 018.
I have 018 after the synthesis of naphthol indole with brompentane also did not crystallize. UR-144, on the contrary, quickly turned into large crystals.

You can always check the result through smoking

 

[Selassi]

Ahahahaha i wouldn't dare smoking bro

 

[Selassi]

A friend will try to spray some cbd-weed with it to test out the potency.

im open for suggestions, tips or different routes who dont require cooling and stuff.

 

[WillD]

If there is no synthesis experience, it is better to start with an intermediate (3-(1-naphthoyl)indole or TCMP-indole for exp). A simple reaction to one stage to the final product. There are suppliers of intermediates.

 

[Selassi]

Yes bro, i did half of the test with already made naph-i and half of the test of my own synthesized naph-i. Both stay in this oily phase.

 

[G.Patton]

Have you tried crystallize it in freezer or dry in vacuum desiccator? Sometimes you need rub product by glass rod to make crystallization centers. Also, you can try to recrystallize from another solvents. Crystallization of organic product is difficult procedure sometimes.

 

[Selassi]

Yes im gonna try the different methods near the end of week. Thank you.
Ill keep everybody updated

 

[BoonDock]

Yes im gonna try the different methods near the end of week. Thank you.
Ill keep everybody updated

SelassiHow was the potency? It was still good was it not? I had some of this oily sticky stuff before and it worked great.

 

[MrSung]

Are there other other additional processes that could be carried on to the ur-144 inorder to increase it potency?