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VAPE LIQUID THC

Curiousonion

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Ok, will do it tomorrow.
It's a very simple reaction and all the chemicals are easy to obtain. Gives a 86% d8. Yield is close to 100%
 

Curiousonion

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To a 5liter 2 neck flask add

1:1 ratio of cbd isolate /methanol (1 liter methanol 1 kilo cbd)
Bring to 63c
Add 1% p-acid
Reflux for 60 minutes (gentle)

Let cool down.
Add 2 liters dcm

Do water wash
Bicarb wash
Another water wash
Separate water from dcm

Distill dcm
Short path distillation to get clean product
 

GOUPIL

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thank you so much for your help!

i don't understand well theses parts :
Bring to 63c
Add 1% p-acid

Can you give me your mail in case of the forum is down or crash?
 

Curiousonion

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You mix the cbd with the methanol and you raise the temp to 63c. Once it reaches that you add 1% p acid by volume to the cbd then you reflux it for an hour
 

GOUPIL

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thank you for all your post! i am trying something and i will keep you in touch !
 

CristalKing

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To a 5liter 2 neck flask add

1:1 ratio of cbd isolate /methanol (1 liter methanol 1 kilo cbd)
Bring to 63c
Add 1% p-acid
Reflux for 60 minutes (gentle)

Let cool down.
Add 2 liters dcm

Do water wash
Bicarb wash
Another water wash
Separate water from dcm

Distill dcm
Short path distillation to get clean product
What is p-acid ? ( phosphoric acid ??) and how many delta 9 and delta 8 is after this reaction ?
 

Curiousonion

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What is p-acid ? ( phosphoric acid ??) and how many delta 9 and delta 8 is after this reaction ?
It's p-Toluenesulfonic acid. 86% delta 8. No delta 9.
To get d9 you need to use a different method.
 

OKS1945

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You can find the same set on alibaba.com probably for a few hundreds dollars or something.
 

Curiousonion

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All equipment should be bought from china. Saves you a ton of money
 
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