DET synthesis (and analogues DMT, DiPT, MiPT) from indole via LiAH. Video manual.

[Novator]

Great video! I seem to recognize the production value and style from somewhere .
Anyway, the MTBE reagent is a bit hard to obtain, is it possible to replace with something less obscure? Or do you have any tip on a good OTC source of it?

DocXEt₂O (diethyl ether) - is an equivalent replacement for MTBE.

Proportions:

20g indole + 300ml anhydrous Et₂O
22g oxalyl chloride + 300ml anhydrous Et₂O

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this is an amazing video! hope to see more

When it's possible, we make video for most popular chem reactions. New videos coming soon

 

[花谢花开]

Et₂O (diethyl ether) - is an equivalent replacement for MTBE.

Proportions:

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When it's possible, we make video for most popular chem reactions. New videos coming soon

NovatorNice to meet you 1. Hello, I would like to ask, does the reflow for 16-26 hours need to be heated? What is the heating temperature? Thank you. Please reply and thank you. 2 In the thread of making 5-meo-dipt, can methyl tert-butyl ether be used as a solvent? I will always look forward to your reply, otherwise I will not be able to sleep. Please reply so that I can sleep well. Thank you very much. a person who needs help

 

[G.Patton]

so if in my garage there is not temperature under 10° i can't start synthesis?

Hank ShraderYou have to use A/C. Correct temperature is significantly important for some substances handling.

 

[花谢花开]

You have to use A/C. Correct temperature is significantly important for some substances handling.

G.PattonCan methyl tert-butyl ether be used instead for the final stage of washing?

 

[G.Patton]

Can methyl tert-butyl ether be used instead for the final stage of washing?

花谢花开I don't know for sure, dioxane can be used instead or petroleum ether.

 

[花谢花开]

You have to use A/C. Correct temperature is significantly important for some substances handling.

G.PattonI saw you posted a new tutorial but I am still interested in this. Hello, can I ask one more question? Is it possible to use methyl tert-butyl ether as a solvent when making 5-meo-dipt on this thread? 2. Approximately what temperature does the reflow need to be heated to for 16 to 26 hours?

 

[G.Patton]

I saw you posted a new tutorial but I am still interested in this. Hello, can I ask one more question? Is it possible to use methyl tert-butyl ether as a solvent when making 5-meo-dipt on this thread? 2. Approximately what temperature does the reflow need to be heated to for 16 to 26 hours?

花谢花开Hello again. Thanks for kind words. As I said, I cannot say for sure concerning methyl tert-butyl ether as a solvent, I guess it will be not so good idea. You can carry out an experiment in a small scale.
So far as temperature concerned, it is temperature, when the mixture is boiled (mostly depends on a used solvent boiling point).

 

[花谢花开]

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