- Joined
- Feb 12, 2022
- Messages
- 84
- Reaction score
- 83
- Points
- 18
4,8g PseudoE
2,5g RP
6g I2
1,5ml H3PO4
oil bath
4 Hours Reflux
after reaction:
150ml DH2O
add NaOH PH 12+
100ml Xylene
wash with warm, cold DH2O
separate funnel
+20ml DH2O
+20ml DH2O
add 35%HCL PH 7
evaporate in heat
washed with cold Acetone
recrystalization in Isopropylalcohol with acetone
left in the freezer for 12 hours
filtered
2,5g RP
6g I2
1,5ml H3PO4
oil bath
4 Hours Reflux
after reaction:
150ml DH2O
add NaOH PH 12+
100ml Xylene
wash with warm, cold DH2O
separate funnel
+20ml DH2O
+20ml DH2O
add 35%HCL PH 7
evaporate in heat
washed with cold Acetone
recrystalization in Isopropylalcohol with acetone
left in the freezer for 12 hours
filtered
Attachments
-
XJswKGMT5C.jpg1.4 MB · Views: 441
-
h6NTuMU9c1.jpg1.4 MB · Views: 376
-
AoBEpviq6s.jpg1.4 MB · Views: 380
-
wcmBvEnA4k.jpg1 MB · Views: 375
-
2yvJkLaSHj.jpg1.7 MB · Views: 369
-
V7CgynN6zT.jpg1.2 MB · Views: 387
-
R92LqAJQPy.jpg956.9 KB · Views: 388
-
kbuSEiX5y9.jpg1.3 MB · Views: 378
-
idVobEk7If.jpg992.9 KB · Views: 377
-
kCYHLs0enK.jpg976.2 KB · Views: 355
-
pwtzxRqfnO.jpg3 MB · Views: 382
-
fhjSBtEpuK.jpg1,021.8 KB · Views: 368
-
ZDlSX8JICA.jpg976.6 KB · Views: 346
-
uPUnhYj2Lv.jpg3.7 MB · Views: 387
-
tZJ7pqXHy4.jpg1.1 MB · Views: 362
-
cEz8puGhKy.jpg1,013.2 KB · Views: 364
-
d6k7xp8ZDh.jpg800 KB · Views: 347
-
PDwZmgzcB3.jpg1 MB · Views: 349
-
pFEbv91fc3.jpg1.3 MB · Views: 386
-
lQxwqtUAbJ.jpg1.1 MB · Views: 369
-
sPqpUCg0lc.jpg804 KB · Views: 378
-
OFkr1tYRE9.jpg1.2 MB · Views: 410
-
UpXZjaf12N.jpg810 KB · Views: 396
-
GQJauexbD4.jpg1.2 MB · Views: 430
Last edited: