Hi sorry for incomplete info
500 g main ingredient (brownish powder
450g pc
255g 5br1pent
1.5 l dmf
main ingredient,pc and dmf together in rm with constant steering,and riaing temperature to 70-75°
I also added 5br1pent slowly in one hour.
-constantly stearing and keeping temp at 75° for another 4h.
total reaction time 5h.
-After 5h i let it cool to room temperature.
-i prepared a bucket with 2 ice water ant 5 kgs of ice
-slowly put the liquid in the bucket and steering with a stick.
-after 5 minutes brownish cristal apear(like a clay)
-everything seems ok ,i put it to dry for a day or two(small ,medium chunks of powder remaining).
For testing i soaked in acetone,2g in 100g of tabacco but the effect was very mild.