Help please for the synthesis of proiony chloride and 4'-Methylpropiophenone

[TucoSalamanca.]

proiony chloride
If you are distilling propionic acid and benzoyl chloride, you need to monitor the temperature closely. Propionic acid has a boiling point of about 141 °C, while benzoyl chloride has a boiling point of about 197 °C. Under reduced pressure, you can distill these compounds at lower temperatures, but the specific pressure will depend on the desired boiling point.

For efficient separation, you may consider distillation under reduced pressure (e.g., about 50-100 mmHg) to avoid decomposition or unwanted side reactions while achieving a lower boiling point for propionyl chloride. Be sure to always perform such reactions in a well-ventilated fume hood and follow appropriate safety protocols.
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In the synthesis of 4‘-Methylpropiophenone I use toluene zinc chloride propiony chloride how many degrees should I distil how many mmhg should I vacuum pump 4’-Methylpropiophenone boiling point 240 degrees
Distillation
The240 °C at standard
Vacuum
The50-100 mmHg.
Example Dist
Distillation Temperature**Dist100-120 °C under reduced
Vacuum Pressure**50-100 mmHg during dist
Summary
Distill100-120 °C under a50-100 mmHg to effectively pur
Is artificial intelligence telling the truth about pressure and distillation?

 

[Dr. MMX]

Man please. I recommended you the proper way for that. Doing this requires knowledge what to do, its not just puting methylamine into bromo ketone like it usually requires to do synethsis and thats all.
You can calculate its boiling point depending on the pressure you provide in system and by referencce informations about chemicals you work.
Simply just find some book and undesrtand the whole process.
You can find some information about processes you will perform on libre texts,
book id: 93154

About the compounds and reaction itself... i suggest just reading organic chemistry book - its very pleasurable.
I have uploaded it. You can find

All you need to do is start by reading, read about distilation process. 1h ago you wanted to distill it at 240c... while its no point to do that, instead you use vacuum distilation. I suggest just reading about these process so you can enjoy the rest when you know what to do.


Instead you pasted that and opened new topic with question if its correct?
The proper way is doing yourself and learning something so next time you will know more.
Do you know what propionyl chloride is and what safety percusions you should perform?

 

[Dr. MMX]

please i even found chapterr that is interesting you in that case
chapter 21st. bbzzzsvqcrqtki6umym6itiixfhni37ybtt7mkbjyxn2pgllzxf2qgyd.onion/resources/organic-chemistry-second-edition-jonathan-clayden-nick-greeves-stuart-warren.4762/

 

[TucoSalamanca.]

normal link send

 

[Dr. MMX]

 

[Dr. MMX]

whats wrong with the link? if you dont use tor version, go into chemical libary and find my listing.

 

[Osmosis Vanderwaal]

Are we talking about propoinyl chloride? Oh hell, this is insane level difficulty. Don't so this in the house guy!

 

[TucoSalamanca.]

It doesn't seem difficult at all.

 

[Osmosis Vanderwaal]

I should have said insane level dangerous for a not chemist

 

[Osmosis Vanderwaal]

The difficult part is getting the stuff to do it I think. Proprionic acid I've heard is terrible stuff. I have a bottle here I don't dare open. The difficulties besides acquiring the chemicals is the caustic nature of them. Not considering how to maintain your life on this earth and also the stench of your neighborhood is where I see the difficulty. You need a plan, a back up plan and a backbackup plan. That fan blowing out your window might now be enough, when you have to leave the room because you eyes are bleeding, that when the reaction gets hot and exceeds the vessel, and you can't get within 20 feet of it because the fumes and the vessel explodes and the curtains come alive with flames, that when you need a backpack up plan. What could you dump on this to put a fire out? Find out first and have it there. What if you burnt your hand? You can't just leave it there running, have a plan. I've got nerves of steel and if I didn't I'd have burnt my house down 5 times, when the alcohol splashes on your hand and you hand lights on fire, you better not drop that beaker!

 

[TucoSalamanca.]

see friends I want to know the pressure and distillation temperature I have a lot of synthesis experience

 

[Dr. MMX]

now i got a proof you didnt even bother to read a very short book that would explain everything to you

 

[TucoSalamanca.]

?

 

[Dr. MMX]

You are incredible dude.

I told you in the start that its only one way to know it urself

 

[TucoSalamanca.]

sorry