1. Procedure
In a 5-l. round-bottomed flask, fitted with a stopper holding a reflux condenser and separatory funnel, are placed 500 g. (10 moles) of powdered sodium cyanide (96–98 per cent pure) and 450 cc. of water. The mixture is warmed on a water bath in order to dissolve most of the sodium...
MethylBenzylPiperazine HCl (MBZP HCl) can be made from Benzyl Chloride (BZC) and MethylPiperazine (MP) in Ethanol by heating it for 30 minutes. Then cool it to 0°C to make MBZP HCl crystals and powder. The extra Methyl group on the other N should prevent Alkylation on the other side.
MethylPhenylPiperazine can be made using MethylPiperazine and Benzyl Chloride by adding them to 99% Ethanol and heating it to 65°C in a hot water bath for 30 minutes to 120 minutes. Then, you can crystallize the MethylBenzylPiperazine HCl.
The chemical reaction of MethylPiperazine and Benzyl...
Benzyl magnesium chloride can be prepared from Benzyl chloride in diethyl ether with a small iodine crystal. Grignard reaction on Acetaldehyde Methylamine yields Methamphetamine. Acetaldehyde Methylimine is prone to polymerization, so it must be used quickly. Grignard reaction on Acetone...
Take pure to Toluene and synthesize Benzyl Chloride by adding TCCA (trichloroisocyanuric acid) and putting it in sunlight and using lithium bromide as a catalyst. Getting benzyl chloride might take hours to days. The lithium bromide makes it go faster so it could take hours instead of days.. You...