mda synthesis

I was looking at a route with good yields, the scarecrow route, but in this route we only have the first part of the synthesis, which would be helional + dmso + hydroxylamine and sodium hydroxide as a base, after cooking for 90 minutes at 85 degrees we add 30% hydrogen peroxide, after that we...

Hey i was just looking around the threads and want to share my experience with this synthesis ( as i didn't find any report for this in moderate scale ) I HAVE DONE THIS PROCEDURE ABOUT 4 TIMES BY NOW AND WOULD LIKE TO SHARE SOME OF IT. EQUIPMENT USED 500ML FLAT BOTTOM FLASK 500mm ALLIHN...

Hi! Attempts at the one-pot Helional to helionamide process, without successful results. Issues seem to be the same some people encountered, so if you can give some hindsight it’d be greatly appreciated: - 13,5g hidroxilamine are added to 175ml DMSO, heating and stirring until it’s dissolved...

Stage 1. α-methyl-1,3-benzodixole-5-propanal oxime The process way presented on Scheme 1. Scheme 1 Starting reagents and materials: 260 g Helional or Ocean propanal (3-(1,3-Benzodioxol-5-yl)-2-methylpropanal CAS 1205-17-0) 400 ml EtOH (Ethanol 88%) 300-350 ml Na2CO3 (107 g Na2CO3 in 300-350...

Introduction Helional [CAS 1205-17-0] is rather interesting substance, which can serve as MDA precursor in the represented simple synthesis. In addition, it has opportunity to become a new MDMA precursor in case MDA conversion to MDMA. BB Forum team are working on this issue after recent China's...

Introduction: A certain vendor online (that shall not be named) appears to be suggesting a "novel" route to phenethylamines. The reaction from aldehyde to amine occurs in 3 distinct steps: 1) A Baylis-Hillman reaction is first used to couple an aryl aldehyde with acrylamide using a tertiary...