1. C

    How to convert from PMK ethyl glycidate (CAS: 28578-16-7) to MDP2P (CAS:4676-39-5)?

    I would like to know how to convert from PMK ethyl glycidate to MDP2P, thanks everyone!
  2. T


    in the synthesis of piperonal and nitroethane, Could I replace it with nitromethane?
  3. V

    Video of MDP2P synthesis

    Hello guys I have a question: There was a video of a complete synthesis of MDP2P in the category video. But now it is gone! Does anyone know the reason why and where I can find or download it from? Thank you very much for any kind of help.
  4. H

    28578-16-7 To mdp2p help

    This is so frustrating. I’ve followed processes to the T and first i yielded a resist clear oil, this second time distilling under vac not exceeding 106c I yielded a totally clear liquid which smells like solvents. idk anymore. Here’s some pics of after adding the pmk oil to 300 ml of naOH...
  5. T0lek511

    From Black Pepper To MDMA Theory

    Hi, This is my first big project in organic chemistry. So your help is welcome. My theory is isolate a piperine from black pepper and convert to a piperic acid. And reaction with potassium permanganate cause a oxidative cleavage and makes piperonal and piperonylic acid (Is possible this acid...
  6. G.Patton

    MDMA synthesis via NaBH4 from MDP2P

    Introduction The following method shows that the NaBH4 reduction actually is superior to all other common routes used in clandestine chemistry and this method allows to scale MDMA synthesis unlike aluminum amalgam reduction. The method is quite simple, it doesn't take expensive equipment...
  7. D

    MDMA Synthesis From Pure PMK Oil

    Hello, I've recently come across a local connection who's able to provide me with [~92%] PMK oil. I've been reading various PMK -> MDMA synth guides on here and other forums, however I'm finding myself asking more questions than the guides are answering. Somebody recommended I try Bright...
  8. G.Patton

    MDP2P (PMK) total synthesis via Safrole

    Introduction These precursors, are controlled or regulated substances in many jurisdictions. The use of uncontrolled precursors therefore offers clandestine laboratory operators a strategy to reduce the risk associated with detection. Catechol (1) is a common chemical reagent that is synthesized...
  9. William Dampier

    MDMA synthesis via Pt/H2. Small scale.

    Reaction scheme: Reagents: Methylamine 40% aq (cas 74-89-5) 2 ml; Ethanol (EtOH) 5 ml; 3,4-Methylenedioxyphenylpropan-2-one (MDP2P; PMK; cas 4676-39-5) 2 ml; Adams' catalyst (PtO2; cas 1314-15-4) 0.05 g; Distilled water 165 ml; Hydrochloric acid (36% aq HCl); Dichloromethane 450 ml; Dodium...
  10. William Dampier

    MDMA synthesis from piperonylmethylketone (PMK/MDP2P) with formic acid

    Reaction scheme: Equipment and glassware: 100 ml round bottom flask; Retort stand and clamp for securing apparatus (optional); Reflux condenser; Heating plate; Funnel; Syringe or Pasteur pipette; pH indicator papers; Beakers (250 mL x2, 100 mL x4); Vacuum source; Laboratory scale (0.01-100 g...