reductive amination

  1. R

    PLEASE HELP! Water bath and rotovap questions…

    Hey guys, I have a synth coming up (currently waiting for the main reagent) and the synth calls for both a water bath and rotovap. So to put my situation into perspective it’s important to say that I am learning chemistry as a hobby and I do not make things for people other than myself! Okay...
    • Rabidreject
    • Thread
    • dmt help reductive amination rotovap steam bath tryptamine vacuum pump
    • Replies: 11
    • Forum: Laboratory FAQ
  2. G

    Amphetamines via Al/Ga reductive amination Al/Hg alternative

    hey folks, to encourage a more ecological sustainable method for amine reduction than Al/Hg, i want to present you the aluminium-gallium-amalgan method. Basically you can just use al-ga amalgan instead the mercury one and that's it. Actually a ratio of 1:1 between reactant and amalgan, while a...
  3. BlueDex

    Synthesis of EthylAmphetamine by non-toxic Aluminum Galinstan amalgam in 70%+ ethanol water using Formic acid, P2P, EtNH2, and Palladium on carbon!

    Hello. You can put Phenyl-2-Propanone (P2P), excess Ethylamine freebase, 70% Ethanol water, some Formic acid, H2CO3 (Seltzer water, Carbonic acid), and Palladium on carbon in a ice cooled round bottom flask or flat bottom boiling flask. Male sure the pH is around 4 and use the pH indicators. You...
    • BlueDex
    • Thread
    • a/gainsn aluminum galinstan non-toxic aluminum galinstan amalgam palladium on carbon pd/c reductive amination synthesis of amphetamine synthesis of ethylamphetamine synthesis of propylhexedrine
    • Replies: 1
    • Forum: Amphetamines (Phenylethylamines)
  4. BlueDex

    Possible MDMA and MDEA synthesis from safrole.

    You can get safrole and hydrate it using dilute phosphoric acid to get MDP2Pol (3,4-MethyleneDioxyPhenyl-2-Propanol). If you use dilute sulfuric acid, the MDP2Pol will rearrange into MDP1Pol (3,4-MethyleneDioxyPhenyl-1-Propanol). Then, you can use manganese dioxide or PCC to oxidize it to MDP2P...
  5. BlueDex

    Methiopropamine synthesis

    Chloroform can react with chlorine gas and iron powder to form carbon tetrachloride and forms hydrogen chloride as a byproduct. Thiophene is brominated to 2-Bromothiophene with bromine in Carbon Tetrachloride. 2-Bromothiophene can react with ethyl acetoacetate and sodium ethoxide and using...
    • BlueDex
    • Thread
    • 1-(2-thiophenyl)-2-propanone bromination carbon tetrachloride chloroform copper (i) iodide enolate methylamine reductive amination
    • Replies: 2
    • Forum: Amphetamines (Phenylethylamines)
  6. L

    Help : Nitrostyrene > 2C-H> 2C-B

    Well Howdy there folks! There’s a lot of info and conversations and loosely, reliable syntheses on many forums discussing using 2 particular reagents, but I need something objective. I’m looking for this “gold standard” synth everyone is having success with using Sodium Borohydride and...
  7. T

    Sodium triacetoxyborohydride (STAB) Synthesis

    NaBH4 is added to RBF and suspended in DCE or THF 3 molar equivalent Glacial acetic acid are added drop wise and the mixture was stirred until no more Hydrogen gas evolved. and after this can I vacuum distillate solvent with little heat and take it to dryness?
    • Tryptamine
    • Thread
    • nabh4 reductive amination sodium triacetoxyborohydride
    • Replies: 0
    • Forum: Tryptamines
  8. BlueDex

    Ethylamphetamine synthesis!

    Take pure to Toluene and synthesize Benzyl Chloride by adding TCCA (trichloroisocyanuric acid) and putting it in sunlight and using lithium bromide as a catalyst. Getting benzyl chloride might take hours to days. The lithium bromide makes it go faster so it could take hours instead of days.. You...
    • BlueDex
    • Thread
    • aluminum amalgam aluminum galinstan amalgam benzyl chloride ethylamine grignard reaction non-toxic aluminum galinstan amalgam phenyl-2-propanone reductive amination toluene
    • Replies: 0
    • Forum: Amphetamines (Phenylethylamines)

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