3,4mdp2np reduction

[amieri]

Hope all is well with everyone . Id like to gather some peoples opinions.
I don't ever come across much on MDA purification on this forum or any of the others. Although similar to amphetamine in many ways I have read unlike amph MDA can't be steamed distilled , if this is true my first question is. What is the science behind why it can't be ?
Now let's say mdp2np was reduced via al/hg , basing to a ph of 11 and collection/drying "mgs04" what do y'all like to do? Directly salting with acetone/h2so4 has lead to some really waxy questionable product. Recrystallation in IPA twice left a fluffy white powder.
My next thought was vacuum distillating the solvent off then resolving in acetone and salting same as before which left a still somewhat waxy product that recrystallized same as before.
Id like to try a/b washing and fractional distillating of the fb.my question is with 10 gram reductions of propene do I need a micro distillation set? Also how does the fb come over? Is it a bumping/jumping type thing or will it actually turn to a vaper ? Any pointers,tips or suggestions are greatly appreciated.
You all please stay amazing and be safe.thanks in advance

 

[HIGGS BOSSON]

We will soon have a video on the synthesis of MDA from helional, and there we will show the methods of purification.
As far as I remember, the processes with MDP2np went the same way as with p2np

 

[amieri]

I check every morning for it ,can't wait higgs you all are such inspirations thanks for being u