I wanted to tell you my first experience in the production of amphetamine sulfate through A-Oil. I have done it through three different processes obtaining practically the same result with a production of around 75%. We are talking about a product without cut and totally dry.
Then I will detail you a little as I have achieved the ingredients and then explain the processes. With this I would like the wise men of the forum to be critical with me and explain what things can be improvable and which unnecessary or implementation.
******************** INGREDIENTS ********************
- A-Oil: supplied by a good reputation forero. I made an initial purchase of 100 cl. To start my tests.
- Sulfuric acid (H2SO4): Obtained by a local sales product that is used to reduce the pH of the swimming pools, it contains 15% of H2SO4. Prepare it in two stages:
1. Evaporation: in a glass flask spotted 2 L. of the content letting it evaporate until I reach the 300 ml mark I did before putting it to heat. Another indicator that I used and with which I am finally going to handle is because of the temperature and it is because while the solution contains a large amount of water, it will not exceed 103 or 104 cº and we will observe when we are close to the 300 ml mark. As that temperature begins to rise slowly. Well, when the mixture reached a temperature of ± 310ºC I turned it off.
2. Distillation: Through a distiller I warmed the mixture between 350 and 370 ºC and with this I could obtain the final H2SO4 solution. My indicator to know that it was quite concentrated was to pour drops into a piece of paper napkin and when this drop made a hole in about 12 seconds to start saving the content.
This process was something dangerous since the solution had very strong boiling episodes which made the flask jump with the danger of breakage and splashes. I managed to mitigate a little by glass of crystals and pieces of broken flasks but still very dangerous. Do you have any remedy to mitigate this reaction more effectively?.
- Methanol: bought as burn alcohol but as the only ingredient the methanol. As I did not see, I distilled it at a temperature of 70ºC.
- Acetona: bought in a local store at 99.5%
******************** PROCESS ********************
1. Diluting and blending 20 ml of A-Oil in 20 ml of acetone at room temperature. To this mixture I was adding drops of a 1/10 solution of H2SO4 and acetone until the pH reached a value of 6.
2. Diluting and blending 20 ml of A-Oil in 100ml of methanol at room temperature. To this mixture I was adding drops of a 1/5 solution of H2SO4 and methanol until the pH reached a value of 6.
3. Diluting and blending 20 ml of A-Oil in 100ml of methanol cooled in the freezer. To this mixture I was adding drops of H2SO4 until the pH reached a value of 6. later I let it cool in the freezer conveniently covered for 12 hours.
Conclusions:
Production almost nothing with a result of about 15 gr. In the three processes. I don't know if production or quality can be increased in some different way. What do you think of all this the wisest teachers in the forum?.
I hope this can also serve new people who are also starting as much as to solve ideas and raise them.
Thanks for all.
Then I will detail you a little as I have achieved the ingredients and then explain the processes. With this I would like the wise men of the forum to be critical with me and explain what things can be improvable and which unnecessary or implementation.
******************** INGREDIENTS ********************
- A-Oil: supplied by a good reputation forero. I made an initial purchase of 100 cl. To start my tests.
- Sulfuric acid (H2SO4): Obtained by a local sales product that is used to reduce the pH of the swimming pools, it contains 15% of H2SO4. Prepare it in two stages:
1. Evaporation: in a glass flask spotted 2 L. of the content letting it evaporate until I reach the 300 ml mark I did before putting it to heat. Another indicator that I used and with which I am finally going to handle is because of the temperature and it is because while the solution contains a large amount of water, it will not exceed 103 or 104 cº and we will observe when we are close to the 300 ml mark. As that temperature begins to rise slowly. Well, when the mixture reached a temperature of ± 310ºC I turned it off.
2. Distillation: Through a distiller I warmed the mixture between 350 and 370 ºC and with this I could obtain the final H2SO4 solution. My indicator to know that it was quite concentrated was to pour drops into a piece of paper napkin and when this drop made a hole in about 12 seconds to start saving the content.
This process was something dangerous since the solution had very strong boiling episodes which made the flask jump with the danger of breakage and splashes. I managed to mitigate a little by glass of crystals and pieces of broken flasks but still very dangerous. Do you have any remedy to mitigate this reaction more effectively?.
- Methanol: bought as burn alcohol but as the only ingredient the methanol. As I did not see, I distilled it at a temperature of 70ºC.
- Acetona: bought in a local store at 99.5%
******************** PROCESS ********************
1. Diluting and blending 20 ml of A-Oil in 20 ml of acetone at room temperature. To this mixture I was adding drops of a 1/10 solution of H2SO4 and acetone until the pH reached a value of 6.
2. Diluting and blending 20 ml of A-Oil in 100ml of methanol at room temperature. To this mixture I was adding drops of a 1/5 solution of H2SO4 and methanol until the pH reached a value of 6.
3. Diluting and blending 20 ml of A-Oil in 100ml of methanol cooled in the freezer. To this mixture I was adding drops of H2SO4 until the pH reached a value of 6. later I let it cool in the freezer conveniently covered for 12 hours.
Conclusions:
Production almost nothing with a result of about 15 gr. In the three processes. I don't know if production or quality can be increased in some different way. What do you think of all this the wisest teachers in the forum?.
I hope this can also serve new people who are also starting as much as to solve ideas and raise them.
Thanks for all.