Dear Chemists - Who synthesizes A-PVP Tell me how to correctly Aminate Bromovalerophenone with Pyrolidin. What is the temperature and time of the reaction?
Correct Amination of A-PVP
- Thread starter Himik
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Alpha-PVP synthesis (1-10kg scale). Complete video tutorial.
Introduction This topic is represented alpha-PVP synthesis way in a medium scale 1-10 kg. There are elaborated video tutorials, which are allowed to produce this substance to anybody. Also, you can find here a list of necessary equipment and reagents. Equipment and glassware: Round bottom...
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Quote
3. A drop funnel tap is opened and pyrrolidine is added dropwise with vigorous stirring.
4. The temperature is maintained below 65 ℃.
5. The reaction mixture is vigorously stirred for 1 hour after completion of the pyrrolidine addition.
