Hello
I am a new beginner please guide me
1.Methylamine gas (MeNH2) 300 g is dissolved in chilled 3000 g methanol (MeOH; -17-20 °C) in 20 L reactor, equipped with thermometer and overhead stirrer. The mixture is cooled down to 5 °C. The stirrer is turned on and MDP2P 1000 g is added.
Does this step require a reflux condenser?
2.The mixture is stirred for 2 days. The stirring time can be reduced to 4 h for people in a hurry, 10-20% will be lost.
After adding all the sodium borohydride (NaBH4), we can reduce the stirring time to 4 hours right now?, can I do the next step? or must complete 48 hours
Thank you very much for your help.
I am a new beginner please guide me
1.Methylamine gas (MeNH2) 300 g is dissolved in chilled 3000 g methanol (MeOH; -17-20 °C) in 20 L reactor, equipped with thermometer and overhead stirrer. The mixture is cooled down to 5 °C. The stirrer is turned on and MDP2P 1000 g is added.
Does this step require a reflux condenser?
2.The mixture is stirred for 2 days. The stirring time can be reduced to 4 h for people in a hurry, 10-20% will be lost.
After adding all the sodium borohydride (NaBH4), we can reduce the stirring time to 4 hours right now?, can I do the next step? or must complete 48 hours
Thank you very much for your help.