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@btcboss2022 bro, what is your suggestion for final crystals washing for the lay people, if acetone is not available in the country?
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@btcboss2022 bro, what is your suggestion for final crystals washing for the lay people, if acetone is not available in the country?
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orgasmatron"Now for my question, does one have to separate MDMA enantiomers to produce big, glassy crystals?"
wrong. one separated isomers (s or d no matter ) not give you big glossy crystal. here is the difference of mdma from meth.
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I have used Ethyl Acetate and Acetonitrile for recryst. many times but only for cleaning meth ( not creating crystals as described)
Using Ethyl Acetate, I have never been able to fully dissolve 100% at boiiling point, no matter how much excess I used. Still, it leaves behind very clean meth, especially the small percentage that in fact crystalizes out after initial solution is filtered and filtrate put in the freezer. Acetonitrile does dissolve everything ( I dont know the usual ratio but as soon as I have an opportunity I'll take notes to share) but it does not remove all the colorizing impurities by itself, but if one adds activated charcoal and filters through celite in a large porous hot glass buchner ( no filter paper, so that it can run quickly)(otherwise it can and will solidify within the pores and clog the entire thing, mix with celite precipitates, create a real real mess, my advice is to experiment before scaling up).
Now for my question, does one have to separate MDMA enantiomers to produce big, glassy crystals?
wrong. one separated isomers (s or d no matter ) not give you big glossy crystal. here is the difference of mdma from meth.