- Language
- 🇨🇿
- Joined
- Feb 22, 2025
- Messages
- 55
- Reaction score
- 11
- Points
- 8
I would need some advice. I'm already desperate. Some time ago, I reacted normally and it was always good as a result. Then I didn't do it for a while and when I came back the results are very bad and I don't know what I'm doing wrong. I'm using Nurofen Stop Grip. The pesudeoephedrine I get is white, it probably won't be a problem. I cook in an oil bath and use a ratio of pseudo-1g/0.5g phosphorus/1g iodine and 0.4ml H3po4. I heat the pseudo phosphorus and H3PO4 to a temperature of 110C, then I start throwing in the iodine, which I divide into 10 equal parts and throw in every two minutes. I finish after 20 minutes at a temperature of 130C. then I hold the reaction for another 20-30 minutes at a temperature of 130C, the reaction happens there, the bubbles are there. Everything looks like before, but the result is weak and the smell is different. I tried replacing the chemicals with new ones.. It didn't help, I tried a different ratio of substances, it didn't help either. I've been struggling with this for a long time, so if anyone can advise me I'll be very grateful