Hello Sodium ethly sulfate synthetic

[TucoSalamanca.]

water does not crystallize, I do not understand, it does not crystallize

 

[wael gano]

After removing the water from the freezer, are there crystals?

 

[TucoSalamanca.]

please help me with this synthesis

 

[wael gano]

How do people help you when you did not mention anything about the reagents used and what you did
Check the reagents

 

[TucoSalamanca.]

Ethanol Absolute >99.5
97-98% Sulfuric Acid

 

[wael gano]

How much acid and ethanol did you add?
How much water did you add?
Next time no one answered you, I told you to mention the synthesis in detail so that you know what is wrong with this

 

[TucoSalamanca.]

In the neutralization part, I added about 70, 80 or 100 ml of water, then I added 50 ml of distilled water, ie 200 ml of ethanol, 100 ml of sulfuric acid to crystallize.

 

[wael gano]

There must be salt crystals if the reagents are correct
Make sure of that

 

[wael gano]

Send a picture of the reagents you used
Make sure you have added sodium carbonate

 

[TucoSalamanca.]

dude i evaporated the solution i got the powder thanks for everything

 

[wael gano]

Make sure that it may have decomposed due to the heat. Take the sodium nitrite part, make a distillation, and check the condenser, if there are any nitro ethane drops.

 

[TucoSalamanca.]

96% ethanol, at what temperature should I reflux and how many ml of ethanol and how many ml of sulfuric acid should I use?

 

[TucoSalamanca.]

the job is done

 

[HerrHaber]

U sure?

 

[TucoSalamanca.]

after reflux I neutralized, then basified, then evaporated

 

[HerrHaber]

you mean reflux to neutralize, then alkainize, I HOPE IN ORDER TO TRIPLY EXTRACT with a sep funnel then dried well over anh. MgSO4>decant > concentrate=> (solvated form of demoniac protodraconic incepts>useful incepts.)