Amphetamine from P2P (phenyl-2-propanone)
- Thread starter G.Patton
- Start date
Bad news no reaction at all like my previous 4 fails
when all the water is removed from my light yellow substance, the pH is back 7
I try to wash with NaOH so pH is back 14 but when separated again pH is back 7
after add methanol1/1 and dropwise sulphuric acid zero reaction nothing
this is now the 5th time the last step fail
PS: my light yellow substance smelt very good
Saul my man, no offense but if you can't perform your steam distillation it's not the syntheses fault or people are not lying to you. According to your description you destroyed the freebase by heating it so much that water instantly evaporated, it is plain wrong what you did.If you care to stop improvising tried and tested techniques like steam distillation maybe you would get more results. Either add some clean water to the extracted portions in 1 vessel, or with 2 separate vessels, 1 for steam connected to the other one.
Solvents recovery
Introduction In the synthesis of mephedrone (4-MMC) and other psychoactive substances at different stages (synthesis and purification) use different solvents, which are not entered into a chemical reaction. They remain in the same form as before syntheses. However, they are mixed with dirt, and...
bbgate.comSteam Distillation
Introduction. Steam distillation is analogous to simple distillation, the main difference being that steam (or water) is used in the distilling flask along with the material to be distilled. Experimentally the setups are arranged more or less the same (Fig.1), with small differences being how...
bbgate.comDecantation, gravity filtration and liquid transferring
Introduction. In this topic, I'll overview some important laboratory techniques. Hard to overestimate the useful and helpful importance of these operations. Decanting, gravity filtration and liquid transferring are simple but take some attention and a little laboratory skill. Practicing them is...
bbgate.comWill this work if I want to get MDA from M.D-phenylacetone? How does the proccess change? What can I do If I can afford the rotovap? Is there a video explaining the proccess? Sorry for all this questions, I am an undergraduate chemist that wants to start cooking
This is MDA obtained by the leucart reaction.
Good product with a pleasant aroma.
The most interesting thing is that the smell remains even after distillation and washing with acetone
This means that less than 1% of aromatic impurities give an intense smell to the product.
Good product with a pleasant aroma.
The most interesting thing is that the smell remains even after distillation and washing with acetone
This means that less than 1% of aromatic impurities give an intense smell to the product.
- By Bartholomeus
Nice rocks you obtained
You used mdp2p via formamide+formic acid to get mda? standard leuckart reaction?
Does ratios for leuckart amphetamine also work for leuckart mdma-mda reaction?
You used mdp2p via formamide+formic acid to get mda? standard leuckart reaction?
Does ratios for leuckart amphetamine also work for leuckart mdma-mda reaction?
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Conditions are different.
various hydrolysis.
MDMA and methamphetamine can be produced by the leucart reaction.
You need n-methylformamide.
To get huge yields - you must learn to understand the essence of the process and feel the reaction.
various hydrolysis.
MDMA and methamphetamine can be produced by the leucart reaction.
You need n-methylformamide.
To get huge yields - you must learn to understand the essence of the process and feel the reaction.
- By Bartholomeus
What are the yield from MDMA and meth produced by leuckart? 800-900ml from 1L ketone?
What do you mean with various hydrolysis?
And what do you mean with the essence of the process?
What do you mean with various hydrolysis?
And what do you mean with the essence of the process?
What is aluminum grit. can share me whit aluminum grit formula.
