I read a lot of different threads and posts asking and talking about MDMA freebase crystallization methods.
I guess many of them are tested and other ones are only taken from litherature.
I tested some of them and as always I post the most effective in my case and for what I need that dont means that is the BEST method only means that is the BEST one for ME.
Normally I dont like to post detailed methods as this one Im very cautios with them because people used to understand that Im posting the BEST and unique method with all the collateral consequencies that It has, I prefer to post complete and concrete synth not General methods.
Anyway here It is:
1. Add portionwise cold HCL37% to the MDMA freebase(previously cooled too) while stirring until PH 3.
2. Heat the mixture gradually while stirring until 130C
3.Has ready a bucket, with 10 times the volume of initial freebase, of freezed acetone that has been at least 48 hours in freezer
4. When mixture is at 130C stop heating and pour It fast in the acetone bucket with vigorously stirring.
5. Leave the bucket in the Freezer at least 72 hours.
6. Take out the bucket and Filter solids with vacuum until It get dry, at the final part of that process pour a small amount freezed acetone over the solids to wash them before totally dry. The filtered acetone is keep It in the Freezer to try to crystallize more material if nothing else crystallized you can let the acetone dry at RT in a flat plate or similar to recover material or freebase
7. Once is completely dried Crush it and convert all into powder.
8. Solve the powder in distilled hot water(1gr/1ml).
9. When all the powder is solved Heat the mixture until 112C with some stirring and throw It fast into the cristallization bucket choosen.
10. Leave the bucket in a "calm" place, no Air flow, no movements, vibrations... At least 48 hours at RT after 48 hours put It 30 min in the Freezer before Filter It.
11. Filter the crystals and wash them with freezed acetone, the filtered liquid is saved to add It in the step 9 in the Next batch.
I Hope this method could solve most of crystallization issues that you could and the questions sent too.
I would like to clarify again that is not the BEST method or the unique one, Its just one more there are a lot of methods and techniques Im just posting the more appropiate for me, for my case and for my circumstances.
Thanks.
I guess many of them are tested and other ones are only taken from litherature.
I tested some of them and as always I post the most effective in my case and for what I need that dont means that is the BEST method only means that is the BEST one for ME.
Normally I dont like to post detailed methods as this one Im very cautios with them because people used to understand that Im posting the BEST and unique method with all the collateral consequencies that It has, I prefer to post complete and concrete synth not General methods.
Anyway here It is:
1. Add portionwise cold HCL37% to the MDMA freebase(previously cooled too) while stirring until PH 3.
2. Heat the mixture gradually while stirring until 130C
3.Has ready a bucket, with 10 times the volume of initial freebase, of freezed acetone that has been at least 48 hours in freezer
4. When mixture is at 130C stop heating and pour It fast in the acetone bucket with vigorously stirring.
5. Leave the bucket in the Freezer at least 72 hours.
6. Take out the bucket and Filter solids with vacuum until It get dry, at the final part of that process pour a small amount freezed acetone over the solids to wash them before totally dry. The filtered acetone is keep It in the Freezer to try to crystallize more material if nothing else crystallized you can let the acetone dry at RT in a flat plate or similar to recover material or freebase
7. Once is completely dried Crush it and convert all into powder.
8. Solve the powder in distilled hot water(1gr/1ml).
9. When all the powder is solved Heat the mixture until 112C with some stirring and throw It fast into the cristallization bucket choosen.
10. Leave the bucket in a "calm" place, no Air flow, no movements, vibrations... At least 48 hours at RT after 48 hours put It 30 min in the Freezer before Filter It.
11. Filter the crystals and wash them with freezed acetone, the filtered liquid is saved to add It in the step 9 in the Next batch.
I Hope this method could solve most of crystallization issues that you could and the questions sent too.
I would like to clarify again that is not the BEST method or the unique one, Its just one more there are a lot of methods and techniques Im just posting the more appropiate for me, for my case and for my circumstances.
Thanks.
