P2NP AL/HG SUURES MAHUS

pdwshopnl

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Kuidas mõtlete selle eksotermilise reaktsiooni skaleerimisest?
Loomulikult leian lahenduse, ei ole sõna ,,selle võimatu".

Ma mõtlen lisada valmis amalgamaadi AL portsjoniteks reaktsioonianumasse.
Näiteks 1kg p2np reduktsioon, kõik alumiinium on vaja 1-1,2KG. See AL :4 portsjonit = 250-300grammi igaühele. Ja esimene AL portsjon valmistatakse hgcl2-ga, dekanteeritakse vesi ja lisatakse kogu reaktiivid anumasse, pärast stabiliseeritud reaktsiooni 30-40min lisatakse järgmine portsjon AL amalgaamitud, 30-40min järgmine AL portsjon.
Mida te arvate IT kohta?
 

pdwshopnl

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Loomulikult räägime tööst hdpe-tünnis, mille peal on mehaaniline segisti koos enda valmistatud suure kondensaatoriga, ja väljaspool tünni kokkutõmbamine
 

William D.

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Mitte suuri portsjoneid korda, vaid lisage tilguti P2NP lahust segades ja jahutades. Kondensaatori kasutamine tünni jaoks annab tulemuse, kuid peamine kontroll välise temperatuuri üle.
 

michelAMPH

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Als ik de Almagaam toe voeg aan de Isopropanol.
Dan de P2NP oplos in Azijnzuur 80% vervolgens die langzaam druppel in de Almagaam/Isopropanol oplossing zou dat werken?
 

w2x3f5

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In this case, there will be more intermediate products, or the amalgam will have to be kept in acetic acid.
 

w2x3f5

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The portioned addition of purified aluminum and mercury salt, and amalgaming directly in the reactor, mercury nitrate looks better than chloride. An important nuance, amine must be distilled in a vacuum in order to eliminate any mercury compounds in the product as much as possible.
 

William D.

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The distillation of alcohol, which will remain after the reaction, will also allow you to get the best yield.
 

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But it will not completely solve the problem of residual amounts of mercury compounds in the product.
 

michelAMPH

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Dank jullie wel!!
Kwik nitraat is hier niet te krijgen alleen chloride.
Aan eind product was ik altijd standaard 2/3 keer met Isopropanol 99,9.
en laat het zeker geen pasta!
 
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