Question good vacuum pump for short path distillation and rotovap

mycelium

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What is the best pump to buy, to be used both for a short path distillation set up, and for a roto...probably even filtration. I don't want to spend 2 grand on the pump, but it has to do the job, and do it right...
I know some syntheses say to use reduced pressure, but some say to distill under 40mm Hg which is close to a full vacuum and probably not going to happen with a 100$ HVAC pump.
One that comes with a roto , in this picture, uses water in the bottom of the pump to make a vacuum...do you think it will get down to 40mm Hg?
Thank you
ECcSmnl2M6
 

mycelium

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Don't want this post to disappear.
Can you tell me what this kind of pump is called, with water down below
And won't cold water make it more vac, in which case it wouldn't do a real vac all the time...
I am going to look at the vacuum guys post...
 

ruen

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have you heard of chatgpt? its this new cool ai thing kids are using to pretend they are smart

To compare 1.33 mbar and 40 mmHg, we need to convert them to the same unit. Let's convert 40 mmHg to mbar:

Conversion factors:

  • 1 mmHg ≈ 1.33322 mbar
So:
40 mmHg × 1.33322 mbar/mmHg ≈ 53.33 mbar
Now compare:

  • 1.33 mbar vs 53.33 mbar

Interpretation:

  • Lower pressure means a better (stronger) vacuum.
  • 1.33 mbar is much lower than 53.33 mbar, so:
✅ 1.33 mbar is a stronger (better) vacuum than 40 mmHg.

No, 40 mm Hg is not close to a full vacuum.
Here’s why:

  • Atmospheric pressure at sea level is about 760 mm Hg.
  • A perfect vacuum is defined as 0 mm Hg (complete absence of pressure).
  • So 40 mm Hg still represents a significant amount of pressure—about 5.3% of atmospheric pressure remains.
In vacuum terms:
  • 40 mm Hg absolute pressure = 720 mm Hg vacuum (since vacuum is often measured relative to atmospheric pressure).
  • That would be called a partial vacuum, but not a "high vacuum".
  • High vacuum typically starts below 1×10⁻³ mm Hg (or 0.001 mm Hg), and ultra-high vacuum is much lower.
Conclusion:
40 mm Hg is a moderate vacuum—not close to a full (or perfect) vacuum.

check this post to learn more https://bbgate.com/en/threads/providing-and-application-of-vacuum-in-a-laboratory.813/
nevertheless, apparently a simple water aspirator can reach 32 mbar. you could also use that circulating water to cool your condenser. and it is propably cheaper as well. my suggestion would be to get one of those instead.
 

Osmosis Vanderwaal

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1.33322mnbar represents the rotary evaporator above this contraption, this vacuum pump/condensor pump says 0.098 m pa
 

Osmosis Vanderwaal

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Is there something that says the vacuum pumps use the water? I thought there was a vacuum pump and a water pump for the condensor that were not the same apparatus, but it doesnt make clear what kinbd of pump it uses. If it can pull 0.098mbar, that boils water at 7c 44f so you thats pretty good vacuum. about 7350 microns
 
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Osmosis Vanderwaal

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It actually DOES pump them both from the same pump. It's a liquid ring vacuum pump and they work similar to a rotary vein pump, but the outside of the impellors move water so the air pressure is sealed but theres no friction. it has an offset shaft and the pricipal is similar to a rotary vein
 

Osmosis Vanderwaal

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yes, it can get quit a bit lower than 40mm/hg, down to about 8-9mm/hg is the claim. Yes the water temperature affects it, so get that $99 mini ice machine too ( I have one)
 

mycelium

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Well, a chiller comes w the roto, down to -5, but I can make a cooling bath to a lot lower if necc
 
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