Aluminium amalgam (Al/Hg) Summary
Vai to var izmantot, lai aizstātu sintēzes, kurās nepieciešams NaBH4? Es mēģinu izgatavot 5-MeO-DMT no 5-MeO-T pēc Hamiltona Norisa sintēzes, bet man nav pieejams NaBH4.
- By G.Patton
Es tā nedomāju
↑View previous replies…
Vai ir kāds veids, kā izgatavot NaBH4, kam nav nepieciešama īpaši augsta temperatūra vai spiediens un ko var veikt nelielā mērogā amatieru laboratorijā, vai arī man vienkārši padoties un pasūtīt no Ķīnas un cerēt, ka muita mani neapšaubīs?
Kāpēc Al/Hg nedarbojas šajā sintēzē. tam vajadzētu reducēt imīnu, lai metilētu triptamīnu, vai ne?
Domāju, ka tas varētu būt iespējams, bet neesmu pilnīgi pārliecināts. Vai jūs domājat, ka tas samazinās indola dubultsaiti?
Vienīgais, par ko es neesmu pārāk pārliecināts, ir produkts, vai no tā tiks izgatavots MMT vai DMT. Jūsu veiktajā metamfetamīna sintēzē no amfetamīna ar Al/Hg amīnam tiek pievienota tikai viena metilgrupa.
Kā pēc dzīvsudraba šķīduma sagatavošanas slāpekļskābē, pēc tam pievienojot šo šķīdumu kolbai ar ūdeni un alumīnija foliju, pareizi izvadīt šīs reakcijas dūmus? Dūmi šķiet pietiekami spēcīgi, lai izkļūtu no gaisa filtra un izkļūtu arī caur masku. Es domāju izmantot vakuumsūkni ar kolbu, tad vakuuma regulatoru, lai vakuuma stiprums būtu pietiekams, lai izgarojumus varētu izvadīt ārā, bet mani māc bažas par ūdeņraža gāzes sūknēšanu, jo tas varētu radīt sprādziena risku.
Sveiki, vai es varu izmantot tādu pašu dzīvsudraba (Ii) hlorīda daudzumu kā dzīvsudraba (Ii) nitrātu amfetamīna sintēzei pls.
Try doing a test run of amalgam on a small amount and you will see. It is usual to take a little more chloride than nitrate.
But it is not always necessary that the reaction of the mercury salt be very active, many people prefer to put less mercury salt so that the reaction is calmer. It all depends on you and your conditions.
If the reaction is weak, you need more mercury salt, if it's too strong, you need less. Obviously.
But it is not always necessary that the reaction of the mercury salt be very active, many people prefer to put less mercury salt so that the reaction is calmer. It all depends on you and your conditions.
If the reaction is weak, you need more mercury salt, if it's too strong, you need less. Obviously.
I am trying to do an amalgam of 10g aluminum. I have mercuric nitrate as a liquid, 30ml,it is 1.5% mercury and I assume the rest is water. Is this enough, not enough or too much mercury for that 10g aluminum. Can the aluminum be overreacted ? Can I let the aluminum sit in the mercury solution for 24 hrs ? Like if I throw it all together and forget about it for a day till I want to use it, is it storable in the mercury solution, to stay as usable amalgam ?
Explain how you obtained 30 mL of a 1.5% solution of mercury. This is very similar to dissolving metallic mercury in nitric acid. And it's too much for 10 g of aluminum.
If you were planning to put aluminum foil in a flask, pour in water, and add a solution of mercury nitrate, you can't store that solution. The mercury will react with the foil.
If you were planning to put aluminum foil in a flask, pour in water, and add a solution of mercury nitrate, you can't store that solution. The mercury will react with the foil.
↑View previous replies…
A order from some webjoint called Zoro. It’s mercury at 1.5% , nitric acid and water. How much u think 10g aluminum will need ? 10ml ?
Either way I’ll be hawk eyeing the shit so I’ll get it done. In a week hope for good posts of good rxn or wait and see me complain for a week cuz I messed it up somehow lol
Any advice ? I’m trying this one with amalgam and I’m doing the copper synth as well
Either way I’ll be hawk eyeing the shit so I’ll get it done lol. Hope for good posts here in a week, or wait and see me complain for a week cuz I can’t do it right for some reason lol