If you had done your research, you would know the answer to this....
I'll still tell you what a 5 minute Google search would have told you...
3, 4, 5, trimethoxybenzaldehyde to 3,4,5, trimethoxynitrostyrene, 3, 4, 5 trimethoxynitrostyrene to mescaline.
How you get to these I will not electorate on, as you can find that through Google and this website
I'll still tell you what a 5 minute Google search would have told you...
3, 4, 5, trimethoxybenzaldehyde to 3,4,5, trimethoxynitrostyrene, 3, 4, 5 trimethoxynitrostyrene to mescaline.
How you get to these I will not electorate on, as you can find that through Google and this website
Using a primary amine and nitromethane, correct? Oh and then whatever you use to reduce it with…
The question I am after is, what primary amine do most people start with?? I saw a synth on here that uses cyclohexylamine…is there an easy to acquire way of obtaining this or can It be replaced with another is it ‘aliphatic’amine? Or something like that. From what iv read there are two types and I always say the wrong one but yeh.
I am looking to do this also but already, of course, knew the info you said. It’s more the ins and outs…for me at least and I don’t even consider myself amateur standard at chemistry lol
The question I am after is, what primary amine do most people start with?? I saw a synth on here that uses cyclohexylamine…is there an easy to acquire way of obtaining this or can It be replaced with another is it ‘aliphatic’amine? Or something like that. From what iv read there are two types and I always say the wrong one but yeh.
I am looking to do this also but already, of course, knew the info you said. It’s more the ins and outs…for me at least and I don’t even consider myself amateur standard at chemistry lol
Okay that’s useful to me. Nitromethane is hard for me to obtain and so I can’t say i would waste it by using it to make methylamine, however, I have seen a synth from firefighters that looks fairly appealing to me, in terms of OTC-ness.
To be fair; having looked into it I could probably actually just make cyclohexylamine and even have the Zn coming - and I actually just ordered the NiCl(II) as well,
about it….
Probably would get better yields this way - pretty much throughout from synthesis of the primary amine/ catylist if I used cyclohexylamine.
Others have suggested using ammonium acetate as the catylist as well…
I don’t know which way I will swing, it depends how much nitromethane I end up with. I do actually have some nitroethane now though so I’m getting there slowly but surely - setting up my next RXN in terms of aquisition of precursors.
ATM I’m working on the reductive amination of tryptamine to tryptophan but I’m out of cash and need dry ice.
I’m willing to admit i postponed me working in the n,n-DMT synth, so I can afford bits for the next one.
A week today, I get the ice…dry ice that is not any type of speed lol although I suppose in the end I will also make the corresponding TMA
To be fair; having looked into it I could probably actually just make cyclohexylamine and even have the Zn coming - and I actually just ordered the NiCl(II) as well,
about it….Probably would get better yields this way - pretty much throughout from synthesis of the primary amine/ catylist if I used cyclohexylamine.
Others have suggested using ammonium acetate as the catylist as well…
I don’t know which way I will swing, it depends how much nitromethane I end up with. I do actually have some nitroethane now though so I’m getting there slowly but surely - setting up my next RXN in terms of aquisition of precursors.
ATM I’m working on the reductive amination of tryptamine to tryptophan but I’m out of cash and need dry ice.
I’m willing to admit i postponed me working in the n,n-DMT synth, so I can afford bits for the next one.
A week today, I get the ice…dry ice that is not any type of speed lol although I suppose in the end I will also make the corresponding TMA
How about ammonium acetate?
- By Rabidreject
I do mean strictly for the 3,4,5-trimeobenzaldehyde to the corresponding b-nitrostyrene
Yeh I realised about ammonium acetate shortly after reaching for pihkal even if he does poo poo it a bit lol
An interesting YouTube video by chemdelic I think is his name, covered this recently and seemed to make it work nicely - even if he did accidentally add nitroethane to 2,5-DMOaldehyde Instead of nitromethane.
I can’t remember exactly how but he found a way to just pour off the water made in situ…
I can’t remember exactly how but he found a way to just pour off the water made in situ…
