Lowest startup cost/least complicated synthesis method

[fiendmaster]

So far what I have in mind is:
Buy CBD isolate, A4 Zeolite and what I wanted was methanol but that isnt available for me so I assume ethanol as a solvent, CO2 gas.

Mix CBD isolate and Zeolite 1:2 put in an airtight container and replace air with CO2, heat for I dont remember how long right now, but I think at 80C.

Then filter wash with the ethanol solvent and afterwards evaporate the ethanol.

Is this correct and a good idea? Also could someone please describe how the product is affected by different ratios and conditions? Also would the end product of this procedure be an oil that I can put in a cart or do I need to do something else like decarb? I would assume after all the heating it should already be decarbed right?

 

[CCL4 huffer]

bro all of these are the kind that u can find decently pure at ur nearest store but u cant rl cyclise the cbd with co2 just get ptsa or AlCl or hcl or mayby a idea of what ur trying to go for since i can tell u the d9/8 synth cant look easy but can be realy shitty in not clean and not controled conditions (also do some more research since ur fumbling more things around than a 8th grader during a chemistry test )

 

[fiendmaster]

So you are suggesting to use one of these two dry reagents right. In that case what should the ratio of the reagents be and how long should I heat it for? And with those should I use ethanol or something else like DCM or n-heptane?

 

[CCL4 huffer]

tolulene worked best for me and for the ptsa to get d8 a ratio of 1mmol cbd to 2 mmol ptsa while at 50c was pretty good.

 

[CCL4 huffer]

for like 48h+- while under sieves

 

[Blammo]

Might as well just buy concentrate of delta 8. Can get a kilo of comcentrate shipped to your door for about 800 to 1000, not even illegal.

Only applies to us

 

[fiendmaster]

Yeah, not US I would be trying to make it if I could buy it

 

[rotovap5002]

Then if you are in the US you might as well buy a kilo of d9

 

[Blammo]

I dont think one can buy delta 9 concentrate by the kilo like delta 8 or other cannabinoids, at least legally and easily.

You can literally google delta 8 concentrate and legal clear net sites will ship if no issues. I haven't found any places online, clear net and legal, that do so for delta 9.

 

[rotovap5002]

Kush.com used to have d9 distillate but now they dont seem to sell it anymore. Pretty strange

 

[CrNQsT]

Ik heb cbd-isolaat vervanging naar delta-9 thc in 30 min. Omdat de bestaande synthese met zware chemicaliën en 12uur refluxkoken gaat, (tijd- en stroomrovend). Heb ik een groenere synthese bedacht, ook vele malen sneller en schoner.
Het HCl in de synthese is nodig om zijn H+ ionen te hebben, er wordt ook diethylether gebruikt om het mengsel van delta-8 en 9-thc uit het reactiemengsel te isoleren. Vaak is het 60/40 %. Delta 8 en 9 thc, en zitten er sporen in van HCl, diethylether en alcohol. En je zit met stank en afval van HCl, diethylether, alcohol, bakingsoda(used for neutraliseren vd HCl after

 

[CrNQsT]

Het refluxkoken. Ook is alcohol 100% duur en diethylether stinkt en is gevaarlijk.
delta 9 thc is wat je wilt, delta 8 heeft alle nare bijwerkingen.
OK , AMBERLYST24 1:1 CBD ISOLAAT EN n-Heptaan

 

[CrNQsT]

Als oplosmiddel. Deze 3 in een vacuümbestendig glas op een Magneetroerderplaat en onder vacuüm 30min. Laten roeren(in het donker)Als alle h+ ionen afgestaanzijn heeft de amberlyst een andere kleur en weetje dat je synthese klaar is. Hoe groffer je amberlyst korrel hoe beter je het eruit filterd. De n'

 

[CrNQsT]

N-heptaan met delta-9 thc, laat je uitdampen op kamertemperatuur en er blijft witte glinsterende kristallen over, delta-9 thc 98% analysed with HPLC. Als de crystallen maar heel iets verwarmt worden, bv tussen je handen..,krijg je bruine plakkende olie. Succes!