Crystallization of cocaine ''HELP''

WebCarteL77

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Hello my friends, I don't know if this is the right place to ask these questions but let's go, I have 1kg of ''PBC'', I would like to know exactly the process to transform it into cocaine hydrochloride and the amount of solvents that I will use, both for the purification of the base and for the crystallization with Hydrochloric Acid
Thank you in advance!

Below is a photo from PBC
 

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w4ri0uiui

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dissolve in ether add activated carbon (to confirm) filter bubble hcl gas
 

Osmosis Vanderwaal

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you can dissolve it in ether. the next thing you would probably want to do is add distilled water and shake it, seperate the water off into the trash 4-5 times. check the ph and add base if the ph gets low (to keep the cocaine from dissolving into the water at all) to clean the crud out. Then bubbling the hcl
 

Chemtrail

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Hey Osmosis Big Bee :)

Haven't you written a couple of these "cocaine purification w/ acetone" ??

Pretty sure
 

Osmosis Vanderwaal

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I may have eluded to or described some processes, but the credit for them should definitely go to David Lee. He uses acetone extensively in his procedures in "The cocaine users handbook" which is available free in 5 places at least and is everything. If youve read it, you know a lot about cocaine (unless you are forgetful) and it's hard to know much without reading it. It's easy to kmow the theories, but he turns theories into procedures, like, "How much hcl does it take to make base cocain back to hcl? 0.25ml and you should add 0.25ml of methanol iso and 0.25 ml acetone to it, to dilute the acid add the mixture of 0.75ml to your base dissolved in acetone to precipitate the hcl. Now you know how to doit without having to bubble hcl gas or wondering what are the best solvents ratios. if you stir the two liquids vigourously, and dump the acid mixture into the cocaine, and dont stir it at all or one bit more, tomorrow you'll have beautiful equal size crystalls of very very pure cocaine hcl. that x100 in the book
 

Osmosis Vanderwaal

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...and then you could say to me, but there's water in the hcl acid, how much cocaine am I going to lose to the liquid?" and I would say, we used 0.25ml of hcl per gram. Hcl is 37% or whatever percent your using, so it has 37% hcl and 63% h2o. 0.25x63%= 0.1575. Since cocaine dissolves in water at 2g/ml , 0,.1575x2=0.315g. The way you recover that is to base the filtered rm and filter the base cocaine back out again
 
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