Aluminium amalgam (Al/Hg) Summary
Dá sa to použiť na nahradenie syntéz vyžadujúcich NaBH4? Snažím sa vyrobiť 5-MeO-DMT z 5-MeO-T podľa syntézy Hamiltona Norrisa, ale nemám k dispozícii NaBH4.
- By G.Patton
Nemyslím si to
↑View previous replies…
existuje spôsob, ako vyrobiť NaBH4, ktorý si nevyžaduje super vysoké teploty alebo tlak a ktorý sa dá urobiť v malom meradle v amatérskom laboratóriu, alebo to mám jednoducho vzdať a objednať z Číny a dúfať, že ma colníci nebudú spochybňovať?
Prečo Al/Hg nefunguje pri tejto syntéze. mal by redukovať imín na metylovaný tryptamín, nie?
Myslím, že by to mohlo byť možné, ale nie som si tým úplne istý. Myslíte si, že sa zníži dvojitá väzba na indole?
Jedinou vecou, ktorou si nie som príliš istý, je výrobok, či sa z neho bude vyrábať MMT alebo DMT. Pri vašej syntéze metamfetamínu z amfetamínu pomocou Al/Hg sa k amínu pridáva len jedna metylová skupina.
Ako sa po príprave roztoku ortuti v kyseline dusičnej a následnom pridaní tohto roztoku do banky s vodou a hliníkovou fóliou správne odvzdušňujú výpary z tejto reakcie? Zdá sa, že výpary sú dostatočne silné, takže unikajú zo vzduchového filtra a prechádzajú aj cez masku. Uvažoval som o použití vákuovej pumpy s bankou a potom vákuového regulátora, aby bolo vákuum dostatočne silné na to, aby sa výpary mohli vypustiť von, ale obávam sa čerpania plynného vodíka, pretože by mohlo dôjsť k výbuchu.
Dobrý deň, môžem použiť rovnaké množstvo chloridu ortuťnatého (Ii) ako dusičnanu ortuťnatého (Ii) na syntézu amfetamínu pls
Try doing a test run of amalgam on a small amount and you will see. It is usual to take a little more chloride than nitrate.
But it is not always necessary that the reaction of the mercury salt be very active, many people prefer to put less mercury salt so that the reaction is calmer. It all depends on you and your conditions.
If the reaction is weak, you need more mercury salt, if it's too strong, you need less. Obviously.
But it is not always necessary that the reaction of the mercury salt be very active, many people prefer to put less mercury salt so that the reaction is calmer. It all depends on you and your conditions.
If the reaction is weak, you need more mercury salt, if it's too strong, you need less. Obviously.
I am trying to do an amalgam of 10g aluminum. I have mercuric nitrate as a liquid, 30ml,it is 1.5% mercury and I assume the rest is water. Is this enough, not enough or too much mercury for that 10g aluminum. Can the aluminum be overreacted ? Can I let the aluminum sit in the mercury solution for 24 hrs ? Like if I throw it all together and forget about it for a day till I want to use it, is it storable in the mercury solution, to stay as usable amalgam ?
Explain how you obtained 30 mL of a 1.5% solution of mercury. This is very similar to dissolving metallic mercury in nitric acid. And it's too much for 10 g of aluminum.
If you were planning to put aluminum foil in a flask, pour in water, and add a solution of mercury nitrate, you can't store that solution. The mercury will react with the foil.
If you were planning to put aluminum foil in a flask, pour in water, and add a solution of mercury nitrate, you can't store that solution. The mercury will react with the foil.
↑View previous replies…
A order from some webjoint called Zoro. It’s mercury at 1.5% , nitric acid and water. How much u think 10g aluminum will need ? 10ml ?
Either way I’ll be hawk eyeing the shit so I’ll get it done. In a week hope for good posts of good rxn or wait and see me complain for a week cuz I messed it up somehow lol
Any advice ? I’m trying this one with amalgam and I’m doing the copper synth as well
Either way I’ll be hawk eyeing the shit so I’ll get it done lol. Hope for good posts here in a week, or wait and see me complain for a week cuz I can’t do it right for some reason lol