Metoda stresanja in pečenja za 4mmc

SonicNL

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Prvi poskus
 

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kharpa177

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ali mi lahko poveste, kako je kristaliziral... ali ste zmešali aceton s hcl in je kapljalo?
 
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SonicNL

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To je prah 4-MMC po opravljeni sintezi.

Tako je bil videti po kristalizaciji.
 

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kharpa177

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imam mdma freebase, ali lahko oblikujem soli mdma tako, da v hladno freebase kapljam hladen hcl + aceton ? Wickr me: monster466
 

kharpa177

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močno sem zakisal freebase, znižal ph.. ali lahko z dodatkom več acetona povečam ph? moj freebase ima raztopino, ki spominja na sluz
 

SonicNL

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Menim, da lahko to storite z vodikovim kloridom. Nisem prepričan.
 

SonicNL

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Poskusite dodati natrijev bikarbonat v majhni količini in izmerite PH.
 

SonicNL

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Ja, mislim, da bi tudi to šlo
 

kharpa177

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pravilno je tako
 

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SonicNL

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Ne morem pomagati pri tem
 

SonicNL

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Ste poskusili poiskati v drugih razdelkih?
 

HerrHaber

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r. t. pomeni sobno temperaturo, je približek standardnih laboratorijskih pogojev, ki pomenijo temperaturo 20C in tlak okolice 760 mm\Hg. MeNH2 je plin, zato počasneje in bolj po delih ga dodajate, manj ga bo ušlo kot plin (brez skrbi, vedno ga dodajamo v presežku), vendar je bistvo, da je potrebna količina nujna za reakcijo s substratom. Tok je bil glede optimizacije postopka, ki je odvisen od natančnega postopka, ki ga izvajate, zato vam lahko pomagam le, če mi podrobno opišete postopek, kaj ste naredili in kaj se je zgodilo, na podlagi tega lahko ocenim in podam predloge.
 

mocnykutas

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Če hočete dobiti čisti kristal, morate videti tako
 

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RegulierTier

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Imam HCl 30-33%
Ali je to še vedno dovolj?
 

SonicNL

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Uporabite več. Izračunajte razmerja.
 

RegulierTier

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Kako zaprete kozarec?
 
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