4-mmc ethyl acetate

  1. Frit Buchner

    Can I get some eyes on these crystals?

    Whats this look like to you? I did a couple things. I heated ammonium chloride and formaldehyde with an alihn condenser and 110° turndown vacuum fitting on top and vacuum pump for a few hours and let it cool and filtered it. Then I distilled the liquid under vacuum for a couple hours and...
  2. WillD

    Mephedrone (4-MMC) synthesis from haloketone in ethyl acetate. 1-10 kg Scale.

    Reaction scheme: Reagents: 1. 4'-Methylpropiophenone (cas 5337-93-9) 1 kg; 2. Hydrobromic acid 48% 1300 ml; 3. Hydrogen peroxide 35% 750 ml; 4. Sodium/potassium hydroxide 25% (NaOH/KOH) aqueous solution; 5. Distilled water; 6. Ethyl acetate 6 l; 7. Methylamine 40% aq - 2 l; 8. Acetone - 8 l...
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