Hi!
Attempts at the one-pot Helional to helionamide process, without successful results.
Issues seem to be the same some people encountered, so if you can give some hindsight it’d be greatly appreciated:
- 13,5g hidroxilamine are added to 175ml DMSO, heating and stirring until it’s dissolved...
Has anyone tried this exact recipe lately? I know Jesse_pinkman_ did a few years back. But he then went of on a Gallium tangent...
Would love to hear some experiences, lessons, tips, tweaks or tricks? Thanks all in advance.
Microwave (small) scale:
1. Benzaldehyde 100 ml, nitroethane 100 ml...