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Reagents:
Indole (cas 120-72-9) 1000 g;
Dichloromethane (CH2Cl2) 15 l;
Tin(IV) chloride (SnCl4) 2000 ml;
1-Naphthoyl chloride (cas 879-18-5) 1627 g;
Nitromethane (cas 75-52-5) 10 l;
Distilled water 20 l;
Ethyl acetate (EtOAc) 15 l;
Sodium or magnesium sulphate (Na2SO4 or MgSO4);
Equipment and...
WillD Thread
Sep 27, 2021
1-naphthoyl chloride
3-(1-naphthoyl)indole synthesis
cas 109555-87-5
cas 879-18-5
indole
jwh 018
jwh-018
Replies: 35
Forum: Cannabinoids
Reaction scheme:
Reagents:
Indole (cas 120-72-9) 0.117 g;
Aluminum oxide (Al2O3) 1 g;
1-Naphthoyl chloride (cas 879-18-5) 0.286 g;
Sodium carbonate (Na2CO3) 0.16 g;
1-Bromopentane (cas 110-53-2) 0.18 g;
Ethanol (EtOH) 60 ml;
Distilled water;
Equipment and glassware:
Microwave vial 5 ml...
WillD Thread
Jul 21, 2021
1-naphthoyl chloride
cannabinoid
cas 110-53-2
cas 120-72-9
cas 209414-07-3
cas 879-18-5
jwh-018 microwave synthesis
jwh-018 small scale
jwh-018 synthesis
spice
Replies: 91
Forum: Cannabinoids
