Hi, I recently thought of a synthesis idea that could be useful, allowing MDA/MDMA to be formed from helional quite easily. I wanted to share this with you and find out what you think, and if you think that's possible.
The first two steps follow the same principle as for the conversion of...
Hi, after receiving many requests via PM, I am posting my final, fully optimised and OTC protocol for synthesising MDA from helional. This post is the result of more than two years of optimisation and testing.
The synthesis takes place in three steps:
- Oxidation of helional to helionic acid
-...
What is a reliable route to Mda from mdp2np, for batches over 100gram.
aluminum/mg seems straight forward, but not scaleable.
Sodium borohydride is difficult to obtain.
Is the tin and zinc route feasible for Mda?
I was looking at a route with good yields, the scarecrow route, but in this route we only have the first part of the synthesis, which would be helional + dmso + hydroxylamine and sodium hydroxide as a base, after cooking for 90 minutes at 85 degrees we add 30% hydrogen peroxide, after that we...
Hey i was just looking around the threads and want to share my experience with this synthesis ( as i didn't find any report for this in moderate scale )
I HAVE DONE THIS PROCEDURE ABOUT 4 TIMES BY NOW AND WOULD LIKE TO SHARE SOME OF IT.
EQUIPMENT USED
500ML FLAT BOTTOM FLASK
500mm ALLIHN...
The reaction proceeds according to Scheme 1
Starting Reagents and Materials
24 g MDA (free base)
50-55 ml Formic acid ethyl ester (ethyl formate CAS 109-94-4)
100 ml flask
Beakers
Reflux condenser
Heater with stir
Synthesis
Formic acid ethyl ester is added to the MDA free base in the...
I have found several publications demonstrating the conversion of carbonyl to amide in “one pot”. First, the oxime is formed, then it is rearranged using various catalysts (ZnO, CuCl2, Cu(OAc)2...).
The advantage of this approach is that the amide can be obtained in just a few hours, and two...
Hi!
Attempts at the one-pot Helional to helionamide process, without successful results.
Issues seem to be the same some people encountered, so if you can give some hindsight it’d be greatly appreciated:
- 13,5g hidroxilamine are added to 175ml DMSO, heating and stirring until it’s dissolved...
https://bbgate.com/data/xfmg/video/9/9021-a0e37be8afcaf24c6b95f4c35bc9ed19.mp4
NOTE: This is not meant to be a complete set of instructions or a recipe to be followed. These are simply the words written out, presented for clarity and discussion.
* -What kind of music do you like to listen to...
The aim of this post is to summarize several months of research and testing. It would be great if everyone could share their results and their thoughts in order to perfect this synthesis route.
All the reagents I'll be using can probably be found in any hardware store, except for helional...
Uncle Fester. Secrets of Methamphetamine Manufacture. Including Recipes for MDA, Ecstasy and Other Psychedelic Amphetamines. Revised and Expanded. 7th ed. 2005
haiii i havent seen this posted here yet. i stole it from the vespiary, so heres the original thread :3
(i added numbers to make things easier, lmk if i need to fix anything)
There are some very promising, unexplored synthesis routes from alpha-methyl-3,4-methylenedioxypheny-propionamide
to...
Hello,
swim have Piperonal but no nitromethane
so is ist Possible to reduce piperonal to Isosafrol just simple like fe/hcl?
And the other question how can i make formamid from Urea (like Adblue)?
Thank you have a nice day