Good evening.
I want to try this method, becouse evaporation of aqua layer tooks too much time for me, but with DCM. do 3cmc hcl in watter not getting to ice when put in freezer?
I want to try this method, becouse evaporation of aqua layer tooks too much time for me, but with DCM. do 3cmc hcl in watter not getting to ice when put in freezer?
- By G.Patton
Hello, your request is unclear. Please, reformulate it correctly.
- By Dr. MMX
within 12h alcohol + h2o solution in such proportions will be a little like just a gel, or even still liquid. It can be put out in the "correct moment " in case it will be more "like ice" if -18 c is used
If DCM is used for the synthesis, the product can be extracted with H2O after acidification.
I dont know the details, but I think its more optimal to evaporate it under pressure if we have just h2o, rather than putting it before its freezing point, I think it will be still needed to be evaporated.
If DCM is used for the synthesis, the product can be extracted with H2O after acidification.
I dont know the details, but I think its more optimal to evaporate it under pressure if we have just h2o, rather than putting it before its freezing point, I think it will be still needed to be evaporated.