3-CMC perfectionizm

misteroil

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Hello guys,
Maybe someone can help my with this. Im going on big scale. Working on demi+HCL solution. And i cant get clear crystals from first crystalization, i need two more recrystalization to obtain crystals like this, an even then my crystals not white.
Keto: MA : DCM 1:2:3, Demi + hcl solution going til 5-6ph. where could be my problem?
 

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misteroil

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If someone is interested in my methods and experience, let's discuss, I will write more details, about pros and cons, wins and fails.
 

breathing.fire

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What yield You have from 1 kg oil and how long You wait for crystals
 

Dr. MMX

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Crystalisation is purification process. You need to remove pure compund from the mother solution.
 

misteroil

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Yeah i find it out, IPA/ETHANOL do that job :) thanks for you, jessie, patton

I made a distilation aparatus myself, now its crystal clear
 
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