3mmc sythese

Studenttt

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Hello,
I have made 3 mmc white the Sythese of the video, the reaction is also the same and everything went good. I have made nice looking crystals but the effect is not good, I think it is the 2-bromo-3-methylpropiophenone from china.
Have somebody made 3 mmc or had this problem can help me
 

Didi

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Is easy to made the same like 4mmc
 

Didi

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U made mistake in syntheiss is simple tye same when u made 4mmc u can made mistake and u get low powder effect
 

WhalterWhite

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friend tried to do the same synthesis as on 4cmc but now on 2bromo 3 chloro. First came the freebase dark orange, in the case of 2 bromo 4 chloro is bright golden. Then, after acidification, HCL turned black. Does anyone know why? Ph to 5-6
 

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WhalterWhite

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After 10 min
 

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little-flower

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hello"" does anyone have a melting point for the 2bromo3methylpropiophenone?
 

ymaaah

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ymaaah

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nope for 2bromo4methylpropiophenone its 75°C, for 2B3MP its 48°C bro ;D
 

little-flower

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nope for 2bromo4methylpropiophenone its 75°C, for 2B3MP its 48°C bro ;D
ymaaahok" thank you"" are you sure,,I can't find any melting point information anywhere.
 
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