- Joined
- Jan 15, 2023
- Messages
- 1,001
- Solutions
- 3
- Reaction score
- 590
- Points
- 113
So it seems the only things left are the reaction didn't reach the required temps, didn't react long enough or were under/ over protonated by the hcl. I too have failed this synth. Twice, matter of fact, in ethyl acetate. The last time I got crystals that looked right, had the right solvency in multiple solvents, melted at the right temperature and 8s identical to the product I was making except it had 0 potency. I'm making my own methylammonium chloride and refining it. I'm at a loss. The CH³NH²HCl looks different from the ammonium chloride. Puts off flammable gas when neutralized by NaOH+ water.... I don't get it. The 2-b-4-mp burns your eyes out and nose run while smelling like orange liquor. I'm lost too
- Joined
- Dec 17, 2023
- Messages
- 17
- Reaction score
- 3
- Points
- 3
So it seems the only things left are the reaction didn't reach the required temps, didn't react long enough or were under/ over protonated by the hcl. I too have failed this synth. Twice, matter of fact, in ethyl acetate. The last time I got crystals that looked right, had the right solvency in multiple solvents, melted at the right temperature and 8s identical to the product I was making except it had 0 potency. I'm making my own methylammonium chloride and refining it. I'm at a loss. The CH³NH²HCl looks different from the ammonium chloride. Puts off flammable gas when neutralized by NaOH+ water.... I don't get it. The 2-b-4-mp burns your eyes out and nose run while smelling like orange liquor. I'm lost too