did you use ice or dcm extraction, tried this writeup for mdmb-5br-inaca, stir 4h at 80C, but there isnt powder in ice water, only some oil
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- By DABOMB
Perfect temperature for this reaction is between 70 and 80 deg. celsius -- any more, and the workup will be a nightmare, any less, and the reaction will not go to completion, leaving impurities that will also inhibit solid crystallization.
