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5cl-adb success from a new cook

Wrinkler

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I ordered 1 kilogram kit from TGRC that consisted of 4 reagents. I added the 4 reagents into a 5l flask at room temperatures. I then used a over head stirrer to homogenize the solution. After about 5 minutes i used my 5l heating mantle with 2 different temperature measuring devices to raise the temp to 79 celsius for 6 hours with constant agitation. After the 6 hours i let my solution cool to 60 celsius. I then agitated the 5l flask full of solution and poured into a clean ample sized container. I then added 5 liters of very salty water (that had no salt settling at the bottom but looked very salty) to the solution. I added this very slowly as to allow my oily solution to seperate ontop of the dense salt water. I then used a 100ml syringe to extract all of the oil. I put the oil in a large silicon container and allow the oil to crystalized and dry out. Any oil i could not extract ended up drying and floating ontop the salt water and i was able to get this crystal but it did have some salt in the crystal. I obtained 1200 grams from the 1000 gram kit.
 

rcprecursorUSA

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Congrats bro! Were you able to get solid product in the end or was it still oily?

Also would you mind providing the full write-up for the synthesis you followed if you have?
 

osmanik

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Do u have to add the salty solution, why i ask because i never heard that step nor u didn't do it with ice to get the final product
 

William D.

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Ice is used so that crystallization is instantaneous. But you can extract the product in the form of oil and crystallize it after
 

osmanik

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Thank you for the information I'm about to get 5cl-adba that I ordered from the forum
 

Mazerakam

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I search that too bro..
 
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