A start.. But still in need of some help

Sitr1x

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So I've bought a full distillation kit and now have all the main equipment needed to start experimenting, but I'm still stuck on where to start things. Should I try P2NP---->P2P------>Meth?

Or should I try to synthesise something like Mephedrone first?

Could anyone provide me with a solid precursor I can make that will get me going in the right direction or has anyone got a good method to making Nitroethane.

I have the confidence to follow well written instructions and video guides if anyone can help a brother out!??? In desperate need to further my Chem experience.
 

Sitr1x

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Anyone?

Really wanting to learn to make something useful that's not too complex or something that I can make some form of profit from.
 

G.Patton

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Anyone?

Really wanting to learn to make something useful that's not too complex or something that I can make some form of profit from.
Sitr1xHello. Sorry for a long reply. I recommend you to start with 4-MMC cuz it's quite easy synthesis and has a good yield, cheap to produce. What precursors do u have? You can open Listing and look for whatever you need.
 

Sitr1x

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Thanks for your reply G.
I'm certainly interested in making 4-mmc but I want to make the 4-methylpropiophenone myself instead of buying it online.

I have a question on this precursor also, is 2-iodo-4-methylpropiophenone basically the same as 2-bromo-4-methylpropiophenone and can either be used for obtaining 4-mmc?

Will follow the video guide on here shortly for the 2-iodo-methylpropiophenone and let you know how I go.

Thanks mate
 

G.Patton

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I have a question on this precursor also, is 2-iodo-4-methylpropiophenone basically the same as 2-bromo-4-methylpropiophenone and can either be used for obtaining 4-mmc?
Sitr1xYes, just different halogen, reaction the same (mechanism). Iodine, in theory, should be better for this reaction.
 

WillD

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I want to make the 4-methylpropiophenone myself instead of buying it online.
Sitr1xCheaper to buy than to make. If you do it cheaper than sold, you need special industrial equipment.
I have a question on this precursor also, is 2-iodo-4-methylpropiophenone basically the same as 2-bromo-4-methylpropiophenone and can either be used for obtaining 4-mmc?
Yes, but iodoketone is more unstable during storage, less yield is obtained from the same amount of iodoketone than from bromoketone (molar calculation). And the price is higher.
Will follow the video guide on here shortly for the 2-iodo-methylpropiophenone and let you know how I go.
Everything is simple there, the main thing is to separate the copper powder well at the end of the reaction.
 

TheWaterman

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Anyone?

Really wanting to learn to make something useful that's not too complex or something that I can make some form of profit from.
Sitr1xIf you are in the USA I have a market for CAS#96-48-0 of about 2200 liters a month and a waiting list of 5k liters at this point . If you could make this for us in the USA uou will be a very rich man very quickly.
 

MrPiolska

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4mmc is very easy to make no special equipment needed 2-iodo-4-methylpropiophenone You can make it in the microwave and 4mmc in wine bottles, which is a real break bad
 

TheWaterman

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Do you happen to know how to make it, what quality it produces, are you in the USA by any chan. I can get anything I want except this at the moment.
 

Curiousonion

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I sent you the synthesis, if done properly it makes a smooth product with zero chemical smell. Just salty.
 
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