Amphetamine purification by acid-base extraction

[kinkyfeet1]

Hi General Patton, I cant find any resource that shows the final production of the pink adderal pills. If i want to make the pink adderal pills, do i have to follow this instruction specific?Thank you for your time and help.

 

[HIGGS BOSSON]

Hi General Patton, I cant find any resource that shows the final production of the pink adderal pills. If i want to make the pink adderal pills, do i have to follow this instruction specific?Thank you for your time and help.

kinkyfeet1Are you interested in the pink color or the composition of the admiral, which includes different salts of amphetamine and dextroamphetamine?

 

[kinkyfeet1]

Are you interested in the pink color or the composition of the admiral, which includes different salts of amphetamine and dextroamphetamine?

HIGGS BOSSONArent all adderal pills pink color on the market? sorry for my naive question, but i want to look into the production of adderal, and how can i start on that?

 

[kinkyfeet1]

Are you interested in the pink color or the composition of the admiral, which includes different salts of amphetamine and dextroamphetamine?

HIGGS BOSSONI have taken one before and it was super helpful for me to focus. it was a pink pill and 20MG written on it I think. is there anyway i can produce the same thing at home or even in a lab with the right resources?

 

[schoolbuoy]

hey everyone I have a question in regards to basic washing w/ IPA-acetone, not ABE yet.
Q1: is pharmacy 99% IPA not good enough? i know acetone from hardware store is not anhydrogenous,
Q2: was reading crack recipe on erowid and some methods talked about heat lamp to dry/ cure the crack: should that be applied to amphetamine/methamphetamine? in general how long do you let them cure?
Q3: what does geranium smell like? i asked bunch of folks I know and surprisingly no one had answer for me

theres few more but all I can think of atm. cheers good folks.

 

[WillD]

hey everyone I have a question in regards to basic washing w/ IPA-acetone, not ABE yet.
Q1: is pharmacy 99% IPA not good enough? i know acetone from hardware store is not anhydrogenous,
Q2: was reading crack recipe on erowid and some methods talked about heat lamp to dry/ cure the crack: should that be applied to amphetamine/methamphetamine? in general how long do you let them cure?
Q3: what does geranium smell like? i asked bunch of folks I know and surprisingly no one had answer for me

theres few more but all I can think of atm. cheers good folks.

schoolbuoyIPA dissolving product and sometimes it is difficult to crystallize, if you do not use acetone.

 

[Frit Buchner]

hey everyone I have a question in regards to basic washing w/ IPA-acetone, not ABE yet.
Q1: is pharmacy 99% IPA not good enough? i know acetone from hardware store is not anhydrogenous,
Q2: was reading crack recipe on erowid and some methods talked about heat lamp to dry/ cure the crack: should that be applied to amphetamine/methamphetamine? in general how long do you let them cure?
Q3: what does geranium smell like? i asked bunch of folks I know and surprisingly no one had answer for me

theres few more but all I can think of atm. cheers good folks.

schoolbuoyIf you consider that 99% iPad is 1% water than it will dissolve a gram of meth per 100ml that you use. It's not hard to dry it though. You don't need to dry crack it forces water out and dries itself pretty fast. A heat lamp could be helpful if your climate is cold. If you evaporate the solvent too fast you won't get the shards you want. The primary action of crystallization is due to the solubility difference between hot solvent and cold solvent. If you evaporate the solvent you just get powder

 

[rabbitass]

How could I reach a very acidic amphetamine? the reagent test turns red

 

[G.Patton]

How could I reach a very acidic amphetamine? the reagent test turns red

rabbitassHi, over-acidified it. It's obvious. You can wash it by IPA or acetone.

 

[rabbitass]

Hi, over-acidified it. It's obvious. You can wash it by IPA or acetone.

G.PattonCan I get it by washing it with IPA? Could methanol be useful?

 

[G.Patton]

Can I get it by washing it with IPA? Could methanol be useful?

rabbitassYes, you can use IPA. If I said IPA washing, It means that you can use IPA for washing....

No, methanol can't be used.

 

[rabbitass]

Can I get it by washing it with IPA? Could methanol be useful?

rabbitassCould it help me to dissolve a little baking soda in the IPA?

 

[G.Patton]

Could it help me to dissolve a little baking soda in the IPA?

rabbitassFor a what reason? Do you understand that amphetamine is basic substance and you make it free base back by baking soda addition?

 

[rabbitass]

For a what reason? Do you understand that amphetamine is basic substance and you make it free base back by baking soda addition?

G.PattonThe pH is too acidic, it is very painful, cleaning it with IPA reduces the burning but the pH is still too acidic when measuring with test strips

 

[rabbitass]

The pH is too acidic, it is very painful, cleaning it with IPA reduces the burning but the pH is still too acidic when measuring with test strips

rabbitassin my mind dissolve some baking soda slightly increase ph to 6 now it is at ph 1

If I do this cleaning with a little baking soda dissolved in the IPA, could it help me? Or if I clean enough with alcohol will I get a pH of 6? at least 5, look at the test strip just by touching the amphetamine

 

[G.Patton]

in my mind dissolve some baking soda slightly increase ph to 6 now it is at ph 1

If I do this cleaning with a little baking soda dissolved in the IPA, could it help me? Or if I clean enough with alcohol will I get a pH of 6? at least 5, look at the test strip just by touching the amphetamine

View attachment 37582

rabbitassForget about baking soda. Describe me please with all details, how did you carry out an extraction of amphetamine free base from a reaction mixture. How did you acidified it? I need to understand a reason of your problem.

 

[rabbitass]

Forget about baking soda. Describe me please with all details, how did you carry out an extraction of amphetamine free base from a reaction mixture. How did you acidified it? I need to understand a reason of your problem.

G.Pattonbuy the sulphate as is
When I took the first line I saw the stars.
then I measured the pH

 

[G.Patton]

buy the sulphate as is
When I took the first line I saw the stars.
then I measured the pH

rabbitassHave you bought ready made amphetamine sulfate? Was it here? Probably, there is sodium hydrogen sulfate, which isn't soluble in IPA and can make it too acidic. Acid-base extraction is only one option for you.

 

[rabbitass]

Have you bought ready made amphetamine sulfate? Was it here? Probably, there is sodium hydrogen sulfate, which isn't soluble in IPA and can make it too acidic. Acid-base extraction is only one option for you.

G.PattonIs there a place where I explain it in a homely way? I find it difficult to get those chemicals

It would really be the first of my life, I see myself capable of doing it but not of getting the products

 

[Berlin777]

once I tried this method but while adding NaOH solution white precipitate showed up so I was unable to rebase it

 

[Jimmyjohn48]

once I tried this method but while adding NaOH solution white precipitate showed up so I was unable to rebase it

Berlin777Seen similar happen. What was the cause

 

[rabbitass]

once I tried this method but while adding NaOH solution white precipitate showed up so I was unable to rebase it

Berlin777does it refer to something like that? the phases were not separated

 

[rabbitass]

It's salt of an adulterant, which your amphetamine has. Amphetamine salt can't make pH 1 at water. It's an acid. After addition NaOH, this acid formed insoluble salt with Na. You can filter it.

G.PattonCan I use toluene as a solvent instead of DCM or Diethyl Ether? It is impossible for me to get any of those 2 solvents.


No oil was formed, did you filter the water to remove the solid and then try to extract the amphetamine from the water?

Sorry for asking so much, I'm trying to find out everything I can through my means but the information is limited.

 

[G.Patton]

Can I use toluene as a solvent instead of DCM or Diethyl Ether? It is impossible for me to get any of those 2 solvents.


No oil was formed, did you filter the water to remove the solid and then try to extract the amphetamine from the water?

Sorry for asking so much, I'm trying to find out everything I can through my means but the information is limited.

rabbitassHi, don't be sorry.
Yes, you can use toluene.
Yes, procedures are correct. But it seems that there is no amphetamine.

 

[Jimmyjohn48]

Curious… I’ve only finished product 2 ways… HCL/sulfuric gas or L/L extraction with water. Mixing the extraction solvents with DH2O mixing and dropping acid until it reaches proper PH levels then evaporating the water. Will that provide as clean of product as adding the H2SO4/acetone to crystallize?

 

[cooperation]

How to crystallize meth meth oil