Beginer we have to start somewhere and i have question

[vljlchoc]

I both sudafed pill each pill content 60 mg of pseudoéphédrine and 500 mg of acétaminophène i crush and i let about an hour in Hydrate de méthyle than i filter and put away the solid and then i boil the solution until i get kind of oil .. when the oil get coller i start to see something christalized than i filter i woul like to know if its the chlorhydrate of pseudoephédrine ? cause it look similar at the video where u put clorydrate of ephedrin i think i am done first step now next step i would love do the reaction as moscou réaction if someone can explain how to process .. i have muriatique acid .. and purified drainer cleaner with hydrogene peroxide now my solution is withe and its supposed to be sulfuric acid .. i saw a video on youtube to made my own sulfuric acid cause here its hard to find a 98% ..,.. for next step its hard for me to find toluene i hope its not a obligation.

Thank u guys and happy new year

 

[Osmosis Vanderwaal]

Yes, it should be pseudoephedrine hcl, as it was hcl in the pill andnyou didnt deprotonate it. You dont need toluene but you didnt mention anything that is going to reduce ephedrine, which could be as much as 40 things.

 

[vljlchoc]

thks for the respond when u mean déprotonate u talk about reaction ? i dont know witch one use theres so many exemple but i will enumarate what i have ... i have phosphore red, i have iodine i have NaoH, sulfuric and muriatic acid i have acétone, xylene, water ditilled and déionized i have ether pétrolium , peroxyde d'ydrogene and breake cleaner heptane base. do you have an idea witch one it could be the good one for me ?

 

[GhostChemist]

http://bbzzzsvqcrqtki6umym6itiixfhn...e-synthesis-via-p-i2-ephedrine-reduction.104/

 

[vljlchoc]

Thks for the video before déprotonate i will chek with the method