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Heroin purification

G.Patton

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Introduction.

The impurities found in street heroin range from coffee to quinine to glass particles. Most impurities, like coffee, are harmless. You might even like some of them. Coffee, for example, is tasted after injecting heroin that has been cut with it. Some impurities, like glass and maybe even quinine, can be deadly. I strongly encourage you to remove the impurities from the heroin you buy. What follows is a recipe that works despite the fact that it has been widely distributed on the Internet.​

Warning.

This recipe explains a serious chemical process with the resulting risks: accidents made during the process could cause harm in the form of explosions, toxic vapors, and unknown other threats to the safety of the would-be chemist and those in close proximity; even if performed exactly as written, this recipe will not increase the quantity, only the quality of what was already there. As a chemist who has dealt with fentanyl, I wanted to comment on the issue of whether this is a dangerous procedure to use on street "heroin" that actually contains fentanyl.
Plain fentanyl should not convert to anything dangerous via the procedure listed. Unless the high or low pH values associated with the procedure were coupled with prolonged exposure to heat, no modification of fentanyl should occur. Nothing dangerous would be generated, to the best of my knowledge. If the product is a fentanyl analogue like sufentanil, I am unsure of what may happen to some of the more fragile aromatic rings upon exposure to strong acid or base, but I would still assume that nothing dangerous would occur.

However, if the "heroin" did contain fentanyl, two problems would arise trying to use this procedure. First, the hydrochloride salt of fentanyl is insoluble in water, and the extraction procedure would be useless as in several steps the desired product would be discarded. Second, the amount of fentanyl in such a mixture would be very small, probably something like 10 mg in a gram of street heroin. This would be exceedingly hard for a novice chemist to extract, and even harder to use properly. Therefore, if a user suspects they have fentanyl (a short-lived high, less euphoria, very white powder, etc), I would suggest they not try this approach. For regular heroin, I would highly recommend it.

If we suppose that street heroin could be fenantyl+filler excipient to dilute and reduce the potency at the heroin level, and we eliminate the filler, it would be possible to suffer an overdose taking the purified fenantyl. So, before the purification, we must be sure that we have heroin and not fenantyl with TLC or teststrype.
On the other hand, this purification technique is only valid to eliminate non-alkaloid fillers/cuttings. If the 'heroin' contains caffeine, morphine, codeine, cocaine or other alkaloids, those will pass through the purification process with heroin because those react similarly to heroin in an acid base extraction.

You need:
  • gram of diacetylmorphine (heroin),​
  • 13 x 100 mm test tubes X 2,
  • 150 ml beaker,​
  • Petri dish or similar small glass container,​
  • cup hydrochloric acid,​
  • glass eye dropper or pipette,​
  • cup distilled water,​
  • cup ammonium hydroxide (normal, clear household ammonia),​
  • cup ethyl ether (some diesel starting fluids; it’s important to read the label before purchasing),​
  • cup sodium bicarbonate (baking soda),​
  • small container to hold the resulting 200-300 mg of pure heroin.​

Procedure.

Removing Particulate Matter.
The use of cotton for filtration when heroin is cooked before being used is a small attempt at purifying the heroin ingested. But a much better job can be done with a little hydrochloric acid (HCl). Place about a gram of heroin in a small glass container (a test tube is best, but any glassware that will allow mixing will work). Add a couple of drops of 28% hydrochloric acid and allow it to react for a couple of minutes. Next, add 5 ml of distilled water and mix vigorously, so that everything dissolves that can. At this point in the process, the heroine is in solution. The non-soluble material in the container is garbage that you do not wish to ingest. Let the solution sit so that the particulate matter settles to the bottom, and then pipette out the solution, leaving the particulate matter behind. The simplest kind of pipette is an eye-dropper. If a pipette is not available, it is possible to pour the solution out of one container into another, being careful not to allow any of the particulate matter to be transferred.

Removing Soluble Impurities.
Add ammonium hydroxide to the solution, one drop at a time. This will cause a white precipitate to form. Continue adding the ammonium until you are certain that there is no more precipitate being formed. The solution is then gently mixed to assure that the ammonium is evenly distributed. At this point, the solution will have a milky look. The solution is then added to about 100 ml of ethyl ether-a chemical with which great care must be taken, since it is quite combustible. This new solution is then vigorously mixed and left to sit. This will cause the water to settle at the bottom of the container; it is removed with a pipette and then discarded. A mixture of 5 mL of HCl and 5 mL distilled water is created and added to the ethyl ether mixture. This is stirred vigorously for several minutes. Afterwards, a water layer will form at the bottom of the container. You then pipette this out and into a small container such as a Petri dish.

Deacidification
Slowly add baking soda to the solution in the Petri dish. This will cause the solution to bubble. When the bubbling stops, this process is finished. The resulting solution is then air-dried, which yields pure heroin and table salt (NaCl). The salt is harmless and may be ingested a long with the heroin.

Heroin is most commonly enjoyed through injection. Typically, users mix roughly 100 mg of pure powdered heroin with about 10 cc of sterile isotonic water for injection. This mixture is heated to boiling and transferred with a syringe while still hot. Again, this is not going to take care of a fentanyl cut. If fentanyl is present in the heroin, it will become an extremely dangerous substance.

Purifying Heroin Again (optional).

1. Dissolve the street heroin in water.
2. Use the easily available Hydrion pH papers to monitor the pH during this procedure. Add Sodium Hydroxide in solution dropwise while checking the pH. Use a narrow glass or plastic rod to touch a minimum of the drug solution to the paper to avoid loss. Stop when the pH reaches about 9.
3. Extract with chloroform. Chloroform is far superior to diethyl ether in that it is non-flammable and does not present storage problems, where explosive peroxides can be formed. Note: Chloroform is an ideal solvent for heroin, codeine, and most other opiates, with the major exception of morphine which requires a mixed solvent.
4. Separate the chloroform layer and wash with a minimum quantity of cold water: 1-2 ml works well. Evaporate the chloroform, taking care not to burn the residue on the bottom of the beaker. Note: Chloroform is a known carcinogen, so plenty of ventilation(and a respirator) would be advisable. The chloroform is so volatile that this step is actually quite easy to perform.
5. Add a dilute solution of HCl dropwise while stirring with a glass rod. Monitor the pH closely. As the acid is being added, the diacetyl morphine base is being neutralized and converted into the water-soluble hydrochloride salt form.
6. When all the solid material has just dissolved, stop adding the HCl. I found that this takes place around pH 5-6. Note: If one tries to bring the pH all the way up to 7, the free base alkaloid precipitates back out, requiring addition of more HCl.
7. The resulting solution will be in an injectable form; it will now be completely clear, with no colored impurities or particulate matter.

Having clarified this procedure, I would hope that nobody would actually attempt it. To an experienced chemist, this is all so routine that you could do it blindfolded. But I noticed that even the college students in Organic lab class, who had no prior organic chemistry experience, were remarkably clueless around a separatory funnel the first time. This is to say that what is trivial in the hands of an experienced chemist will likely be unusable (at best) and dangerous (at worst) in the hands of an amateur. This chemistry isn't to be played with.
 
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darkmatter7

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Now what if we're starting with the typical European "H#3" which is usually mixed with caffeine and only about 25% pure (last time I tested it)
 

G.Patton

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Now what if we're starting with the typical European "H#3" which is usually mixed with caffeine and only about 25% pure (last time I tested it)
darkmatter7You'll get heroine with caffeine in final stage.
On the other hand, this purification technique is only valid to eliminate non-alkaloid fillers/cuttings. If the 'heroin' contains caffeine, morphine, codeine, cocaine or other alkaloids, those will pass through the purification process with heroin because those react similarly to heroin in an acid base extraction.
 

deeperdive36

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Can you use petroleum ether instead. Also when I added the amonia nothing happened no precipitate came out .. what did I do wrong
 

G.Patton

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Can you use petroleum ether instead. Also when I added the amonia nothing happened no precipitate came out .. what did I do wrong
deeperdive36Hello, I think yes. Probably you added too much ammonia in one portion. It is okay.
 

deeperdive36

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Also can you use a lye solution instead of the amonia? Once all completed is there a way of making the results smokable or is it only iv and insufflated
 

G.Patton

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Also can you use a lye solution instead of the amonia? Once all completed is there a way of making the results smokable or is it only iv and insufflated
deeperdive36Yes, you can.
Once all completed is there a way of making the results smokable or is it only iv and insufflated
I guess, you can smoke it also without problems.
 

ZS.28

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Hello there, a friend of mine spilled some regular juice on some 2-3 grams of heroin, and he wants to purify it, is there an easier method that requires less chemicals? Can he use Acetone? if so how to wash with acetone? or any other tip that might help would be truly appreciated!
 

G.Patton

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Hello there, a friend of mine spilled some regular juice on some 2-3 grams of heroin, and he wants to purify it, is there an easier method that requires less chemicals? Can he use Acetone? if so how to wash with acetone? or any other tip that might help would be truly appreciated!
ZS.28I guess a juice won't affect him too much. Heroin HCl sparingly soluble in acetone.
 

nkd23

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Is it possible too use anything else then chloroform?
 

G.Patton

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nkd23

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are you willing too write one? or too much work?
 

S1NTH3T1C

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Chloroform synthesis

1/2L of bleach in a 1L flask

Chill bleach or add ice

Add 10mL acetone at a 50:1 ratio

Let RM react for 60 min

Chloroform will remain at the bottom.

Separate
 
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