I need help with my first MDMA synthesis. PLEASE

mickael1985

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61-50-7

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H2SO4 + NaCl, you shouldn't try chemistry if you don't know the basics, you're exposing yourself to chemical risks and you're exposing consumers to possible impurities you might leave in the final product. I can only recommend that you study at least the strict minimum in chemistry and try this synthesis later.

Best regards
 

hustlerkid

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I'd recommend extracting your mdma freebase with solvent (toluene or dcm).

Add diluted hcl until ph reaches 6. The mdma hcl will be in the h2o and impurties in solvent.

Seperate h2o and evaporate water until crystals form. If mdma crystals are still dirty crush into fine powder and wash in acetone.
 

TrainWreck

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As hustlerkid said. You shouldnt have to gas hcl for it.

Just the typical A/B extraction method for it. Although I haven't done this synth myself, this is a simple step in many extractions.

Freebase with NaOH or KOH solution. Do several pulls with a polar solvent. Use sep funnel to seperate the pulls. DCM is nice to use since density is greater than water so it will sink.

To salt it, I reccomend splitting your solvent in half so you can have some available if you overshoot your PH.

Then dilute HCl with IPA. Add to solvent drop wise and measure PH until you reach PH 6 using presented litmus paper. If you overshoot add in some of the freebase solution previously set aside. Slowly work through that solution until none is left.

Then can add water to make it pull the salt from the NPS. Seperate water and evaporate.
 

Throw-off

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Laboratory FAQ has a whole thread on Gassing liquids.
 

mickael1985

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hello
When and how much do I add formic acid during the 7 hours?
When I add chloridric acid and I heat to 80° is it reflux heated?
Can I replace diethyl ether with acetic ether?
Could you give me the quantities of products for 2 kg of PMK.

Thank you very much
 

CCL4 huffer

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hello
When and how much do I add formic acid during the 7 hours?
When I add chloridric acid and I heat to 80° is it reflux heated?
Can I replace diethyl ether with acetic ether?
Could you give me the quantities of products for 2 kg of PMK.

Thank you very much
mickael1985i personaly would it max only replace the diethyl with mtbe. and the yield fully depends on how good of a chemist u are if u dont fuck it up id say 80% is probable as a beginner
 
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